Technology Process of Phosphine, tri-7-octenyl-
There total 2 articles about Phosphine, tri-7-octenyl- which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
8-Bromo-1-octene;
With
magnesium; ethylene dibromide;
In
tetrahydrofuran;
at 20 ℃;
Inert atmosphere;
With
phosphorus trichloride;
In
tetrahydrofuran;
Inert atmosphere;
Cooling;
DOI:10.1515/znb-2010-0327
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: potassium tert-butylate / Inert atmosphere
2.1: magnesium; ethylene dibromide / tetrahydrofuran / 20 °C / Inert atmosphere
2.2: Inert atmosphere; Cooling
With
potassium tert-butylate; magnesium; ethylene dibromide;
In
tetrahydrofuran;
DOI:10.1515/znb-2010-0327
- Guidance literature:
-
With
dimethylsulfide borane complex;
In
tetrahydrofuran;
at 0 ℃;
for 0.166667h;
chemoselective reaction;
Inert atmosphere;
DOI:10.1515/znb-2010-0327
