4-Methoxy-2-nitrobenzenesulfonamide

Base Information

Chemical Name:4-Methoxy-2-nitrobenzenesulfonamide
CAS No.:81792-84-9
Molecular Formula:C7H8N2O5S
Molecular Weight:232.217
Hs Code.:
DSSTox Substance ID:DTXSID30588447
Wikidata:Q82481118

Synonyms:4-methoxy-2-nitrobenzenesulfonamide;81792-84-9;4-methoxy-2-nitrobenzene-1-sulfonamide;Benzenesulfonamide, 4-methoxy-2-nitro-;SCHEMBL6038599;DTXSID30588447;GS0946;AKOS000141488;MCULE-1902667988;CS-0247728;EN300-37276;G26549;Z237785054

Suppliers and Price of 4-Methoxy-2-nitrobenzenesulfonamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 5 raw suppliers

Chemical Property of 4-Methoxy-2-nitrobenzenesulfonamide

Chemical Property:

XLogP3:0.3
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:6
Rotatable Bond Count:2
Exact Mass:232.01539253
Heavy Atom Count:15
Complexity:330

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC1=CC(=C(C=C1)S(=O)(=O)N)[N+](=O)[O-]

Technology Process of 4-Methoxy-2-nitrobenzenesulfonamide

There total 5 articles about 4-Methoxy-2-nitrobenzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 4-Methoxy-2-nitro-1-phenylmethanesulfonyl-benzene

: 81792-84-9
4-Methoxy-2-nitro-benzol-sulfonsaeure-⁽¹⁾-amid

Guidance literature:: With ammonium hydroxide; In dichloromethane; at 5 ℃; for 0.5h;
DOI:10.1016/j.bmcl.2006.04.022

Reference yield:

: 22057-42-7
2-Nitro-4-methoxy-1-benzylmercapto-benzol

: 81792-84-9
4-Methoxy-2-nitro-benzol-sulfonsaeure-⁽¹⁾-amid

Guidance literature:: Multistep reaction; (i) Cl₂, aq. AcOH, (ii) aq. NH₃;
DOI:10.1021/jm00338a008

Reference yield:

: 10298-80-3
2-chloro-5-methoxynitrobenzene

: 81792-84-9
4-Methoxy-2-nitro-benzol-sulfonsaeure-⁽¹⁾-amid

Guidance literature:: Multi-step reaction with 3 steps

1: 96 percent / Na₂CO₃ / ethanol; H₂O / 5 h / Heating

2: Cl₂; HOAc; H₂O / 0.25 h / 5 °C

3: 88 percent / aq. NH₃ / CH₂Cl₂ / 0.5 h / 5 °C

With ammonium hydroxide; water; chlorine; sodium carbonate; acetic acid; In ethanol; dichloromethane; water;
DOI:10.1016/j.bmcl.2006.04.022