4-(Benzenesulfonyl)-4-(prop-2-en-1-yl)cyclohex-2-en-1-one

Base Information

Chemical Name:4-(Benzenesulfonyl)-4-(prop-2-en-1-yl)cyclohex-2-en-1-one
CAS No.:81842-31-1
Molecular Formula:C15H16O3S
Molecular Weight:276.35100
Hs Code.:
DSSTox Substance ID:DTXSID00528512

Synonyms:81842-31-1;DTXSID00528512;4-(Benzenesulfonyl)-4-(prop-2-en-1-yl)cyclohex-2-en-1-one

Suppliers and Price of 4-(Benzenesulfonyl)-4-(prop-2-en-1-yl)cyclohex-2-en-1-one

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of 4-(Benzenesulfonyl)-4-(prop-2-en-1-yl)cyclohex-2-en-1-one

Chemical Property:

PSA：59.59000
LogP:3.77510
XLogP3:2.3
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:4
Exact Mass:276.08201554
Heavy Atom Count:19
Complexity:478

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C=CCC1(CCC(=O)C=C1)S(=O)(=O)C2=CC=CC=C2

Technology Process of 4-(Benzenesulfonyl)-4-(prop-2-en-1-yl)cyclohex-2-en-1-one

There total 3 articles about 4-(Benzenesulfonyl)-4-(prop-2-en-1-yl)cyclohex-2-en-1-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 81841-92-1
6,6-(ethylenedioxy)-3-allyl-3-(phenylsulfonyl)cyclohexene

: 81842-31-1
4-allyl-4-(phenylsulfonyl)-2-cyclohexenone

Guidance literature:: With pyridinium p-toluenesulfonate; In acetone; for 3h; Heating;
DOI:10.1021/jo00173a040

Reference yield:

: 5535-48-8
PVS

: 81842-31-1
4-allyl-4-(phenylsulfonyl)-2-cyclohexenone

Guidance literature:: Multi-step reaction with 3 steps

1: 2.) p-toluenesulfonic acid / 1.) benzene, reflux, 28 h, 2.) benzene, reflux, 23 h

2: 1.) NaH / 1.) DMF, 2.) 3.5 h

3: 95 percent / PPTS / acetone / 3 h / Heating

With pyridinium p-toluenesulfonate; sodium hydride; toluene-4-sulfonic acid; In acetone;
DOI:10.1021/jo00173a040

Reference yield:

: 81841-89-6
4,4-(ethylenedioxy)-1-(phenylsulfonyl)cyclohexene

: 81842-31-1
4-allyl-4-(phenylsulfonyl)-2-cyclohexenone

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) NaH / 1.) DMF, 2.) 3.5 h

2: 95 percent / PPTS / acetone / 3 h / Heating

With pyridinium p-toluenesulfonate; sodium hydride; In acetone;
DOI:10.1021/jo00173a040