2,6-Bis(4-phenylphenyl)phenol

Base Information

• Chemical Name: 2,6-Bis(4-phenylphenyl)phenol
• CAS No.: 81979-65-9
• Molecular Formula: C30H22O
• Molecular Weight: 398.504
• DSSTox Substance ID: DTXSID00512496
• Nikkaji Number: J1.938.240K
• Wikidata: Q82371751
• Mol file: 81979-65-9.mol

Synonyms:81979-65-9;DTXSID00512496;[1~1~,2~1~:2~4~,3~1~:3~3~,4~1~:4~4~,5~1~-Quinquephenyl]-3~2~-ol

Chemical Property of 2,6-Bis(4-phenylphenyl)phenol

Chemical Property:

• XLogP3: 8.1
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 4
• Exact Mass: 398.167065321
• Heavy Atom Count: 31
• Complexity: 469

Purity/Quality:

85.0-99.8% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Canonical SMILES: C1=CC=C(C=C1)C2=CC=C(C=C2)C3=C(C(=CC=C3)C4=CC=C(C=C4)C5=CC=CC=C5)O

Technology Process of 2,6-Bis(4-phenylphenyl)phenol

There total 8 articles about 2,6-Bis(4-phenylphenyl)phenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

2,6-Biscyclohexanone (81979-68-2) → 2,6-Bisphenol (81979-65-9)

Guidance literature:

sulfur; In diphenylether; for 3h; Heating;

DOI:10.1055/s-1982-29734

Reference yield:

2,6-dibromoanisole (38603-09-7) → 2,6-Bisphenol (81979-65-9)

Guidance literature:

Multi-step reaction with 5 steps

1: H₂ / Pd-C

2: DMAP / pyridine

3: boron tribromide

With dmap; hydrogen; boron tribromide; palladium on activated charcoal; In pyridine; 1: Suzuki coupling / 4: Suzuki coupling;

DOI:10.1002/adsc.200303070

Reference yield:

[4-(benzyloxy)phenyl]boronic acid (146631-00-7) → 2,6-Bisphenol (81979-65-9)

Guidance literature:

Multi-step reaction with 5 steps

1: H₂ / Pd-C

2: DMAP / pyridine

3: boron tribromide

With dmap; hydrogen; boron tribromide; palladium on activated charcoal; In pyridine; 1: Suzuki coupling / 4: Suzuki coupling;

DOI:10.1002/adsc.200303070

upstream raw materials:

2,6-Biscyclohexanone

2,6-dibromoanisole

[4-(benzyloxy)phenyl]boronic acid

1,3-Bis-2-propanone