1,3,2-Diazaphospholidine, 2-chloro-1,3-diphenyl-

Base Information

• Chemical Name: 1,3,2-Diazaphospholidine, 2-chloro-1,3-diphenyl-
• CAS No.: 82017-87-6
• Molecular Formula: C14H14ClN2P
• Molecular Weight: 276.705
• DSSTox Substance ID: DTXSID90513255
• Wikidata: Q82372961

Synonyms:2-Chloro-1,3-diphenyl-1,3,2-diazaphospholidine;82017-87-6;2-Chloro-1,3- diphenyl-1,3,2-diazaphospholidine;SCHEMBL17596435;DTXSID90513255;SY349327

Chemical Property of 1,3,2-Diazaphospholidine, 2-chloro-1,3-diphenyl-

Chemical Property:

• XLogP3: 4.5
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 2
• Exact Mass: 276.0583131
• Heavy Atom Count: 18
• Complexity: 239

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1CN(P(N1C2=CC=CC=C2)Cl)C3=CC=CC=C3

Technology Process of 1,3,2-Diazaphospholidine, 2-chloro-1,3-diphenyl-

There total 3 articles about 1,3,2-Diazaphospholidine, 2-chloro-1,3-diphenyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

N,N'-diphenylethylenediamine (150-61-8) → chloro-2, N,N' diphenyl-1,3 diazaphospholane-1,3,2 (82017-87-6)

Guidance literature:

With triethylamine; phosphorus trichloride; In dichloromethane; at 0 - 20 ℃; for 2.08333h; Inert atmosphere;

DOI:10.1016/j.poly.2011.04.041

Reference yield:

1,4-diphenyl-1,4-diaza-1,3-butadiene → chloro-2, N,N' diphenyl-1,3 diazaphospholane-1,3,2 (82017-87-6)

Guidance literature:

Multi-step reaction with 2 steps

1: lithium aluminium tetrahydride / diethyl ether / -78 °C

2: triethylamine; phosphorus trichloride / tetrahydrofuran / -78 °C

With lithium aluminium tetrahydride; triethylamine; phosphorus trichloride; In tetrahydrofuran; diethyl ether;

DOI:10.1002/zaac.201100023

Reference yield:

aniline (62-53-3) → chloro-2, N,N' diphenyl-1,3 diazaphospholane-1,3,2 (82017-87-6)

Guidance literature:

Multi-step reaction with 2 steps

2: triethylamine; phosphorus trichloride / dichloromethane

With triethylamine; phosphorus trichloride; In dichloromethane;

DOI:10.1021/om300755j

upstream raw materials:

N,N'-diphenylethylenediamine

aniline

Downstream raw materials:

tert-Butyl-(1,3-diphenyl-2-phenylimino-2λ⁵-[1,3,2]diazaphospholidin-2-yl)-amine

CF₃O₃S^(1-)*C₁₄H₁₄N₂P⁽¹⁺⁾

(3R,4R)-3,4-bis(1,3-diphenyl-1,3,2-diazaphospholidin-2-yloxy)-1-(1-naphthyl)pyrrolidine-2,5-dione

C₂₀H₁₈N₂O₃PS^(1-)*Li⁽¹⁺⁾

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