2-Methoxy-5-methylbenzenesulfonamide

Base Information

• Chemical Name: 2-Methoxy-5-methylbenzenesulfonamide
• CAS No.: 82020-49-3
• Molecular Formula: C₈H₁₁NO₃S
• Molecular Weight: 201.246
• DSSTox Substance ID: DTXSID20358499
• Wikidata: Q82139112

Synonyms:2-methoxy-5-methylbenzenesulfonamide;2-Methoxy-5-methyl-benzenesulfonamide;643087-31-4;82020-49-3;Benzenesulfonamide, 2-methoxy-5-methyl-;2-methoxy-5-methylbenzene-1-sulfonamide;SCHEMBL5188196;DTXSID20358499;AKOS000142241;FS-2350;SB78012;SDCCGMLS-0064898.P001;EN300-270568;AH-487/42822072;SR-01000285013;SR-01000285013-1;Z57611437

Chemical Property of 2-Methoxy-5-methylbenzenesulfonamide

Chemical Property:

• XLogP3: 0.8
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 4
• Rotatable Bond Count: 2
• Exact Mass: 201.04596439
• Heavy Atom Count: 13
• Complexity: 257

Purity/Quality:

85.0-99.8% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC1=CC(=C(C=C1)OC)S(=O)(=O)N

Technology Process of 2-Methoxy-5-methylbenzenesulfonamide

There total 2 articles about 2-Methoxy-5-methylbenzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

p-methylanizole (104-93-8) → 2-methoxy-5-methylbenzolsulfonamid (82020-49-3)

Guidance literature:

With chlorosulphuric acid; chloroform; und Erwaermen des Reaktionsgemisches mit Ammoniumcarbonat;

DOI:10.1021/ja01860a049

Reference yield:

→ 2-methoxy-5-methylbenzolsulfonamid (82020-49-3)

Guidance literature:

With ammonia; water;

DOI:10.1111/j.1553-2712.2001.tb00546.x

Reference yield: 60.0%

2-methoxy-5-methylbenzolsulfonamid (82020-49-3) + phenyl isothiocyanate (103-72-0) → N-2-methoxy-5-methylbenzolsulfonyl-N-phenylthioharnstoff (138686-60-9)

Guidance literature:

for 15h;

upstream raw materials:

p-methylanizole

Downstream raw materials:

N-2-methoxy-5-methylbenzolsulfonyl-N-phenylthioharnstoff

N-2-methoxy-5-methylbenzolsulfonyl-N-allylthioharnstoff

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