Technology Process of 1H-Indene, 5-ethyl-2,3-dihydro-
There total 17 articles about 1H-Indene, 5-ethyl-2,3-dihydro- which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
hydrogen;
platinum(IV) oxide;
In
tetrahydrofuran;
under 1034.3 Torr;
Yield given;
DOI:10.1021/jo00196a024
- Guidance literature:
-
Multi-step reaction with 6 steps
1: thionyl chloride
2: 91 percent / AlCl3 / CS2
3: 89 percent / NaBH4 / ethanol / 25 °C
4: 97 percent / p-toluenesulfonic acid * H2O / benzene / Heating
5: 96 percent / NiCl22 / diethyl ether / Heating
6: H2 / PtO2 / tetrahydrofuran / 1034.3 Torr
With
sodium tetrahydroborate; aluminium trichloride; thionyl chloride; [nickel(II)dichloride(1,3-bis(diphenylphosphino)propane)]; hydrogen; toluene-4-sulfonic acid;
platinum(IV) oxide;
In
tetrahydrofuran; carbon disulfide; diethyl ether; ethanol; benzene;
DOI:10.1021/jo00196a024
- Guidance literature:
-
Multi-step reaction with 8 steps
1: 95 percent / KOH / acetic acid; H2O; tetrahydrofuran
2: 85 percent / 165 °C
3: thionyl chloride
4: 91 percent / AlCl3 / CS2
5: 89 percent / NaBH4 / ethanol / 25 °C
6: 97 percent / p-toluenesulfonic acid * H2O / benzene / Heating
7: 96 percent / NiCl22 / diethyl ether / Heating
8: H2 / PtO2 / tetrahydrofuran / 1034.3 Torr
With
potassium hydroxide; sodium tetrahydroborate; aluminium trichloride; thionyl chloride; [nickel(II)dichloride(1,3-bis(diphenylphosphino)propane)]; hydrogen; toluene-4-sulfonic acid;
platinum(IV) oxide;
In
tetrahydrofuran; carbon disulfide; diethyl ether; ethanol; water; acetic acid; benzene;
DOI:10.1021/jo00196a024
