Benzeneacetic acid, 2-acetylhydrazide

Base Information

• Chemical Name: Benzeneacetic acid, 2-acetylhydrazide
• CAS No.: 82122-73-4
• Molecular Formula: C10H12N2O2
• Molecular Weight: 192.21400
• Hs Code.: 2928000090
• Mol file: 82122-73-4.mol

Synonyms:phenylacetic acid N'-acetyl-hydrazide;N-Acetyl-N'-phenylacetyl-hydrazin;N-acetyl-N'-phenylacetyl-hydrazine;N'-Acetylphenyl-essigsaeure-hydrazid;

Chemical Property of Benzeneacetic acid, 2-acetylhydrazide

Chemical Property:

• PSA: 58.20000
• LogP: 1.17820

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Benzeneacetic acid, 2-acetylhydrazide

There total 2 articles about Benzeneacetic acid, 2-acetylhydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

acetic anhydride (108-24-7) + 2-phenylacetylhydrazine (937-39-3) → N-acetyl-N'-phenylacetylhydrazine (82122-73-4)

Guidance literature:

In acetic acid; for 0.5h;

DOI:10.1007/BF00476205

Reference yield:

→ N-acetyl-N'-phenylacetylhydrazine (82122-73-4)

Guidance literature:

Phenylessigsaeure-hydrazid, Ac2O (Kinetik);

Reference yield: 80.0%

N-acetyl-N'-phenylacetylhydrazine (82122-73-4) + Methyl benzenesulfonate (80-18-2) → N,N'-dimethyl-N-acetyl-N'-phenylacetylhydrazine (137250-37-4)

Guidance literature:

With sodium hydroxide; at 90 ℃; for 0.5h;

DOI:10.1007/BF00476205

upstream raw materials:

acetic anhydride

2-phenylacetylhydrazine

Downstream raw materials:

5-methyl-1-(4-nitrophenyl)-1H-tetrazole

2-benzyl-5-methyl-[1,3,4]thiadiazole

N,N'-dimethyl-N-acetyl-N'-phenylacetylhydrazine

4-phenyl-1,2,3-trimethylpyrazolin-3-one