Benzenemethanaminium, N,N,N-triethyl-, hexafluorophosphate(1-)

Base Information

• Chemical Name: Benzenemethanaminium, N,N,N-triethyl-, hexafluorophosphate(1-)
• CAS No.: 82124-96-7
• Molecular Formula: C13H22N.F6P
• Molecular Weight: 337.289
• Mol file: 82124-96-7.mol

Synonyms:

Chemical Property of Benzenemethanaminium, N,N,N-triethyl-, hexafluorophosphate(1-)

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Benzenemethanaminium, N,N,N-triethyl-, hexafluorophosphate(1-)

There total 6 articles about Benzenemethanaminium, N,N,N-triethyl-, hexafluorophosphate(1-) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

N-benzyl-N,N-diethylethanaminium sulfofluoridate → N-benzyl-N,N-diethylethanaminium hexafluorophosphate(V) (82124-96-7)

Guidance literature:

With potassium hexafluorophosphate; In dichloromethane; water; at 20 ℃; for 24h;

DOI:10.1016/j.tet.2019.07.007

Reference yield: 47.0%

(2,2'-bipyridyl)carbonylbis{μ-(di-p-tolyltriazenido-N(1)N(3))}(triphenylphosphine)dirhodium hexafluorophosphate + N-benzyl-N,N,N-triethylammonium chloride (56-37-1) → (2,2'-bipyridyl)carbonylchlorobis{μ-(di-p-tolyltriazenido-N(1)N(3))}(triphenylphosphine)dirhodium hexafluorophosphate + N-benzyl-N,N-diethylethanaminium hexafluorophosphate(V) (82124-96-7)

Guidance literature:

In dichloromethane; N2 atmosphere; filtn., addn. of hexane, partial evapn. (vac.), filtn. of org compd., concn., crystn. from CH2Cl2-hexane; elem. anal.;

Reference yield: 45.0%

(2,2'-bipyridyl)carbonylbis{μ-(di-p-tolyltriazenido-N(1)N(3))}(P(OPh)3)dirhodium hexafluorophosphate + N-benzyl-N,N,N-triethylammonium chloride (56-37-1) → (2,2'-bipyridyl)carbonylchlorobis{μ-(di-p-tolyltriazenido-N(1)N(3))}(P(OPh)3)dirhodium hexafluorophosphate + N-benzyl-N,N-diethylethanaminium hexafluorophosphate(V) (82124-96-7)

Guidance literature:

In dichloromethane; N2 atmosphere; filtn., addn. of hexane, partial evapn. (vac.), filtn. of org compd., concn., crystn. from CH2Cl2-hexane; elem. anal.;

upstream raw materials:

N-benzyl-N,N,N-triethylammonium chloride

triethylamine

methyltris(benzyloxy)silane