Technology Process of Phosphine, [4-(dimethylphosphino)butyl]diphenyl-
There total 4 articles about Phosphine, [4-(dimethylphosphino)butyl]diphenyl- which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 99 percent / dimethylformamide / 4 h / Heating
2: 98 percent / 20percent aqueous sodium hydroxide / 1 h / Heating
3: 1.) trichlorosilane, triethylamine 2.) 50percent aqueous sodium hydroxide / 1.) toluene, 5 min then reflux, 2 h 2.) toluene, ice cooling, 1 h
With
sodium hydroxide; trichlorosilane; triethylamine;
In
N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 79 percent / toluene / 5 h / Heating
2: 99 percent / dimethylformamide / 4 h / Heating
3: 98 percent / 20percent aqueous sodium hydroxide / 1 h / Heating
4: 1.) trichlorosilane, triethylamine 2.) 50percent aqueous sodium hydroxide / 1.) toluene, 5 min then reflux, 2 h 2.) toluene, ice cooling, 1 h
With
sodium hydroxide; trichlorosilane; triethylamine;
In
N,N-dimethyl-formamide; toluene;
- Guidance literature:
-
With
sodium hydroxide; trichlorosilane; triethylamine;
Yield given. Multistep reaction;
1.) toluene, 5 min then reflux, 2 h 2.) toluene, ice cooling, 1 h;
