Benzenepropanamide, b-[chloro[(4-methylphenyl)sulfinyl]methyl]-N,N-dimethyl-

Base Information

Chemical Name:Benzenepropanamide, b-[chloro[(4-methylphenyl)sulfinyl]methyl]-N,N-dimethyl-
CAS No.:823213-64-5
Molecular Formula:C₁₉H₂₂ClNO₂S
Molecular Weight:363.908
Hs Code.:

Synonyms:

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Chemical Property of Benzenepropanamide, b-[chloro[(4-methylphenyl)sulfinyl]methyl]-N,N-dimethyl-

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
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MSDS Files:: SDS file from LookChem

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Technology Process of Benzenepropanamide, b-[chloro[(4-methylphenyl)sulfinyl]methyl]-N,N-dimethyl-

There total 1 articles about Benzenepropanamide, b-[chloro[(4-methylphenyl)sulfinyl]methyl]-N,N-dimethyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 127-19-5,116057-81-9
N,N-dimethyl acetamide

: 823213-45-2
1-((Z)-1-Chloro-2-phenyl-ethenesulfinyl)-4-methyl-benzene

: 823213-64-5
4-chloro-N,N-dimethyl-3-phenyl-4-(p-tolylsulfinyl)butanamide

Guidance literature:: N,N-dimethyl acetamide; In tetrahydrofuran; at -78 ℃; for 0.166667h;

1-((Z)-1-Chloro-2-phenyl-ethenesulfinyl)-4-methyl-benzene; In tetrahydrofuran; at -78 ℃; for 0.5h;
DOI:10.1016/j.tet.2004.09.113

Reference yield:

: 823213-64-5
4-chloro-N,N-dimethyl-3-phenyl-4-(p-tolylsulfinyl)butanamide

: 1008-73-7
4-phenyldihydrofuran-2(3H)-one

Guidance literature:: Multi-step reaction with 2 steps

1: NaI; trifluoroacetic anhydride / acetone / 0.25 h / -50 °C

2: 98 percent / Bu₃SnH; AIBN / benzene / 0.5 h / Heating

With 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; trifluoroacetic anhydride; sodium iodide; In acetone; benzene; 1: Pummerer cyclization;
DOI:10.1016/j.tet.2004.09.113