6-Heptenoic acid, 7-phenyl-2-[(4E)-5-phenyl-4-pentenyl]-, (6E)-

Base Information

Chemical Name:6-Heptenoic acid, 7-phenyl-2-[(4E)-5-phenyl-4-pentenyl]-, (6E)-
CAS No.:824431-41-6
Molecular Formula:C24H28O2
Molecular Weight:348.485
Hs Code.:

Synonyms:

Suppliers and Price of 6-Heptenoic acid, 7-phenyl-2-[(4E)-5-phenyl-4-pentenyl]-, (6E)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemicals and raw materials
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Total 1 raw suppliers

Chemical Property of 6-Heptenoic acid, 7-phenyl-2-[(4E)-5-phenyl-4-pentenyl]-, (6E)-

Chemical Property:

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 6-Heptenoic acid, 7-phenyl-2-[(4E)-5-phenyl-4-pentenyl]-, (6E)-

There total 6 articles about 6-Heptenoic acid, 7-phenyl-2-[(4E)-5-phenyl-4-pentenyl]-, (6E)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 824431-40-5
(E)-2,2-dimethyl-5,5-bis[(4E)-5-phenylpent-4-enyl][1,3]dioxane-4,6-dione

: 824431-41-6
(6E)-7-phenyl-2-[(4E)-5-phenylpent-4-enyl]hept-6-enoic acid

Guidance literature:: With water; In tetrahydrofuran; at 165 ℃; for 4h; microwave irradiation;
DOI:10.1021/jo0483466

Reference yield:

: 14371-10-9
(E)-3-phenylpropenal

: 824431-41-6
(6E)-7-phenyl-2-[(4E)-5-phenylpent-4-enyl]hept-6-enoic acid

Guidance literature:: Multi-step reaction with 6 steps

1: 71 percent / BH₃*HNMe₂ / methanol / 3 h / 20 °C

2: 90 percent / 1.5 h / 170 °C / microwave irradiation

3: 100 percent / DIBALH / tetrahydrofuran; CH₂Cl₂ / 4 h / -78 °C

4: 89 percent / I₂; PPh₃; imidazole / CH₂Cl₂ / 0 - 20 °C

5: 47 percent / cesium carbonate / acetonitrile / 72 h / 20 °C

6: 74 percent / H₂O / tetrahydrofuran / 4 h / 165 °C / microwave irradiation

With 1H-imidazole; dimethylamine borane; water; iodine; diisobutylaluminium hydride; caesium carbonate; triphenylphosphine; In tetrahydrofuran; methanol; dichloromethane; acetonitrile; 1: Knoevenagel condensation;
DOI:10.1021/jo0483466

Reference yield:

: 72651-96-8,121740-84-9
(E)-2,2-dimethyl-5-(3-phenylallyl)-1,3-dioxane-4,6-dione

: 824431-41-6
(6E)-7-phenyl-2-[(4E)-5-phenylpent-4-enyl]hept-6-enoic acid

Guidance literature:: Multi-step reaction with 5 steps

1: 90 percent / 1.5 h / 170 °C / microwave irradiation

2: 100 percent / DIBALH / tetrahydrofuran; CH₂Cl₂ / 4 h / -78 °C

3: 89 percent / I₂; PPh₃; imidazole / CH₂Cl₂ / 0 - 20 °C

4: 47 percent / cesium carbonate / acetonitrile / 72 h / 20 °C

5: 74 percent / H₂O / tetrahydrofuran / 4 h / 165 °C / microwave irradiation

With 1H-imidazole; water; iodine; diisobutylaluminium hydride; caesium carbonate; triphenylphosphine; In tetrahydrofuran; dichloromethane; acetonitrile;
DOI:10.1021/jo0483466