Benzenamine, 2,4-dimethoxy-5-methyl-

Base Information

• Chemical Name: Benzenamine, 2,4-dimethoxy-5-methyl-
• CAS No.: 82477-59-6
• Molecular Formula: C9H13NO2
• Molecular Weight: 167.208
• Mol file: 82477-59-6.mol

Synonyms:2,4-Dimethoxy-5-methyl-phenylamine;2,4-dimethoxy-5-methyl-aniline;2,4-Dimethoxy-5-methyl-anilin;2.4-Dimethoxy-5-methyl-anilin;

Chemical Property of Benzenamine, 2,4-dimethoxy-5-methyl-

Chemical Property:

• Boiling Point: 139 °C (10 mmHg)
• PSA: 44.48000
• LogP: 2.17560

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Benzenamine, 2,4-dimethoxy-5-methyl-

There total 4 articles about Benzenamine, 2,4-dimethoxy-5-methyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

1,5-dimethoxy-2-methyl-4-nitrobenzene (50342-31-9) → 2,4-dimethoxy-5-methylaniline (82477-59-6)

Guidance literature:

With hydrogen; 10% palladium on activated carbon; In ethanol; ethyl acetate; for 1h; under 2068.65 Torr;

Reference yield:

2-chloro-4,6-dimethoxy-3-methylaniline (82477-57-4) → 2,4-dimethoxy-5-methylaniline (82477-59-6)

Guidance literature:

With hydrogen; triethylamine; palladium on activated charcoal; In ethanol;

Reference yield:

2-methyl-1,4-benzoquinone 4-oxime (13362-33-9) → 2,4-dimethoxy-5-methylaniline (82477-59-6)

Guidance literature:

Multi-step reaction with 2 steps

1: 15.1 g / hydrogen chloride gas / 25 - 30 °C

2: 2.5 g / hydrogen, triethylamine / Engelhard 10percent palladium-charcoal / ethanol

With hydrogenchloride; hydrogen; triethylamine; palladium on activated charcoal; In ethanol;

upstream raw materials:

1,5-dimethoxy-2-methyl-4-nitrobenzene

2-chloro-4,6-dimethoxy-3-methylaniline

2-methyl-1,4-benzoquinone 4-oxime

Downstream raw materials:

1-isocyanato-2,4-dimethoxy-5-methylbenzene