Carbamic acid, [(1S)-2-[[5-(butylamino)-2-hydroxy-1-[(3-hydroxyphenyl)methyl]-4-methyl- 5-oxopentyl]amino]-1-methyl-2-oxoethyl]-, 1,1-dimethylethyl ester

Base Information

• Chemical Name: Carbamic acid, [(1S)-2-[[5-(butylamino)-2-hydroxy-1-[(3-hydroxyphenyl)methyl]-4-methyl- 5-oxopentyl]amino]-1-methyl-2-oxoethyl]-, 1,1-dimethylethyl ester
• CAS No.: 824957-19-9
• Molecular Formula: C25H41N3O6
• Molecular Weight: 479.617

Synonyms:

Chemical Property of Carbamic acid, [(1S)-2-[[5-(butylamino)-2-hydroxy-1-[(3-hydroxyphenyl)methyl]-4-methyl- 5-oxopentyl]amino]-1-methyl-2-oxoethyl]-, 1,1-dimethylethyl ester

Chemical Property:

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MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Carbamic acid, [(1S)-2-[[5-(butylamino)-2-hydroxy-1-[(3-hydroxyphenyl)methyl]-4-methyl- 5-oxopentyl]amino]-1-methyl-2-oxoethyl]-, 1,1-dimethylethyl ester

There total 1 articles about Carbamic acid, [(1S)-2-[[5-(butylamino)-2-hydroxy-1-[(3-hydroxyphenyl)methyl]-4-methyl- 5-oxopentyl]amino]-1-methyl-2-oxoethyl]-, 1,1-dimethylethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

{(S)-1-[(1S*,2S*,4R*)-1-(3-benzyloxybenzyl)-4-butylcarbamoyl-2-hydroxypentylcarbamoyl]ethyl}carbamic acid tert-butyl ester (824957-18-8) → {(S)-1-[(1S*,2S*,4R*)-4-butylcarbamoyl-2-hydroxy-1-(3-hydroxybenzyl)pentylcarbamoyl]ethyl}carbamic acid tert-butyl ester (824957-19-9)

Guidance literature:

With hydrogen; palladium 10% on activated carbon; In ethanol; at 20 ℃; for 4h; under 760.051 Torr;

Reference yield:

{(S)-1-[(1S*,2S*,4R*)-4-butylcarbamoyl-2-hydroxy-1-(3-hydroxybenzyl)pentylcarbamoyl]ethyl}carbamic acid tert-butyl ester (824957-19-9) + tert-butyl 6-bromohexanoate (65868-63-5) → 6-{3-[(2S*,3S*,5R*)-2-((S)-2-tert-butoxycarbonylaminopropionylamino)-5-butylcarbamoyl-3-hydroxyhexyl]phenoxy}hexanoic acid tert-butyl ester (824957-20-2)

Guidance literature:

With potassium carbonate; potassium iodide; In acetone; for 120h; Heating / reflux;

Reference yield:

{(S)-1-[(1S*,2S*,4R*)-4-butylcarbamoyl-2-hydroxy-1-(3-hydroxybenzyl)pentylcarbamoyl]ethyl}carbamic acid tert-butyl ester (824957-19-9) + tert-butyl 5-bromovalerate (88987-42-2) → 5-{3-[(2S*,3S*,5R*)-2-((S)-2-tert-butoxycarbonylaminopropionylamino)-5-butylcarbamoyl-3-hydroxyhexyl]phenoxy}pentanoic acid tert-butyl ester (824957-21-3)

Guidance literature:

With potassium carbonate; potassium iodide; In acetone; for 168h; Heating / reflux;

upstream raw materials:

{(S)-1-[(1S*,2S*,4R*)-1-(3-benzyloxybenzyl)-4-butylcarbamoyl-2-hydroxypentylcarbamoyl]ethyl}carbamic acid tert-butyl ester

Downstream raw materials:

6-{3-[(2S*,3S*,5R*)-2-((S)-2-tert-butoxycarbonylaminopropionylamino)-5-butylcarbamoyl-3-hydroxyhexyl]phenoxy}hexanoic acid tert-butyl ester

5-{3-[(2S*,3S*,5R*)-2-((S)-2-tert-butoxycarbonylaminopropionylamino)-5-butylcarbamoyl-3-hydroxyhexyl]phenoxy}pentanoic acid tert-butyl ester

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