N,N-Diethyl-2-methoxy-4,5-dimethylbenzamide

Base Information

Chemical Name:N,N-Diethyl-2-methoxy-4,5-dimethylbenzamide
CAS No.:82544-94-3
Molecular Formula:C14H21NO2
Molecular Weight:235.326
Hs Code.:
DSSTox Substance ID:DTXSID20577269
Wikidata:Q82467225

Synonyms:N,N-Diethyl-2-methoxy-4,5-dimethylbenzamide;82544-94-3;DTXSID20577269

Suppliers and Price of N,N-Diethyl-2-methoxy-4,5-dimethylbenzamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of N,N-Diethyl-2-methoxy-4,5-dimethylbenzamide

Chemical Property:

XLogP3:2.8
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:4
Exact Mass:235.157228913
Heavy Atom Count:17
Complexity:251

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CCN(CC)C(=O)C1=C(C=C(C(=C1)C)C)OC

Technology Process of N,N-Diethyl-2-methoxy-4,5-dimethylbenzamide

There total 1 articles about N,N-Diethyl-2-methoxy-4,5-dimethylbenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 33500-88-8
1-bromo-2-methoxy-4,5-dimethylbenzene

: 88-10-8
N,N-diethylcarbamyl chloride

: 82544-94-3
N,N-diethyl-(2-methoxy-4,5-dimethyl)benzamide

Guidance literature:: With tert.-butyl lithium; Yield given. Multistep reaction; 1.) hexane, THF, -78 deg C, 5 min, 2.) hexane, THF, RT, 24 h;

Reference yield:

: 82544-94-3
N,N-diethyl-(2-methoxy-4,5-dimethyl)benzamide

: 82544-90-9
N,N-Diethyl-5-formyl-2-methoxy-4-methyl-benzamide

Guidance literature:: With ammonium cerium(IV) nitrate; In water; acetic acid; at 0 ℃; for 1h; Yield given;
DOI:10.1021/ja00381a059

Reference yield:

: 82544-94-3
N,N-diethyl-(2-methoxy-4,5-dimethyl)benzamide

: 138042-04-3
1-(2-methoxy-4,5-dimethylphenyl)-2-methylbutan-1-one

: 138042-05-4
N,N-diethyl-6-methoxy-3,4-dimethyl-2-trimethylsilylbenzamide

Guidance literature:: With chloro-trimethyl-silane; N,N,N,N,-tetramethylethylenediamine; sec.-butyllithium; Yield given. Multistep reaction. Yields of byproduct given; 1.) ether, cyclohexane, -78 deg C, 1 h, 2.) ether, cyclohexane, from -78 deg C to RT, 12 h;