2-(Phenylazo)-M-cresol

Base Information

• Chemical Name: 2-(Phenylazo)-M-cresol
• CAS No.: 29418-38-0
• Molecular Formula: C13H12 N2 O
• Molecular Weight: 212.251
• Nikkaji Number: J1.614.008B
• Mol file: 29418-38-0.mol

Synonyms:2-(PHENYLAZO)-M-CRESOL;29418-38-0;Benzolazo-m-Kresol;2-(Phenylazo)-3-methylphenol

Chemical Property of 2-(Phenylazo)-M-cresol

Chemical Property:

• Vapor Pressure: 0mmHg at 25°C
• Boiling Point: 354.2°Cat760mmHg
• Flash Point: 168°C
• Density: 1.11g/cm³
• XLogP3: 3.7
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 2
• Exact Mass: 212.094963011
• Heavy Atom Count: 16
• Complexity: 236

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC1=C(C(=CC=C1)O)N=NC2=CC=CC=C2

Technology Process of 2-(Phenylazo)-M-cresol

There total 2 articles about 2-(Phenylazo)-M-cresol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-methyl-2-nitrobenzene (88-72-2) + aniline (62-53-3) → 2-hydroxy-6-methylazobenzene (29418-38-0) + 4-amino-phenol (123-30-8) + N-[(2-methylphenyl)imino]benzenimine oxide (34810-71-4)

Guidance literature:

mit Sonnenlicht im geschlossenen Gefaess_.Irradiation;

Reference yield:

N-[(2-methylphenyl)imino]benzenimine oxide (34810-71-4) → 2-hydroxy-6-methylazobenzene (29418-38-0) + 3-Methyl-4-phenylazo-phenol (1435-88-7)

Guidance literature:

With antimonypentachloride; Yield given. Multistep reaction. Yields of byproduct given; 1.) CCl₄, overnight; 2.) nitromethane, 81-83 deg C, 3 h;

DOI:10.1016/0040-4020(80)80162-1

upstream raw materials:

1-methyl-2-nitrobenzene

aniline

N-[(2-methylphenyl)imino]benzenimine oxide