Technology Process of DL-Glutamic acid, N-(diphenylmethylene)-, diethyl ester
There total 1 articles about DL-Glutamic acid, N-(diphenylmethylene)-, diethyl ester which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
tetrabutylammomium bromide; potassium carbonate;
In
acetonitrile;
Ambient temperature;
DOI:10.1016/0040-4020(96)00395-X
- Guidance literature:
-
Multi-step reaction with 4 steps
1: KOH, BrNBu4 / acetonitrile / 0 °C
2: 22 percent / H2 / 10percent Pd/C / ethanol / 2280 Torr / Ambient temperature
3: 95 percent / Et3N, DMAP / CH2Cl2 / Ambient temperature
4: 75 percent / 6M HCl / Heating
With
hydrogenchloride; dmap; potassium hydroxide; tetrabutylammomium bromide; hydrogen; triethylamine;
palladium on activated charcoal;
In
ethanol; dichloromethane; acetonitrile;
DOI:10.1016/0040-4020(96)00395-X
- Guidance literature:
-
Multi-step reaction with 2 steps
1: KOH, BrNBu4 / acetonitrile / 0 °C
2: 22 percent / H2 / 10percent Pd/C / ethanol / 2280 Torr / Ambient temperature
With
potassium hydroxide; tetrabutylammomium bromide; hydrogen;
palladium on activated charcoal;
In
ethanol; acetonitrile;
DOI:10.1016/0040-4020(96)00395-X
