Hydrazinecarboxylic acid, 2-[[2-[(1,1-dimethylethoxy)carbonyl]-1-(2-methylpropyl)hydrazino]acetyl]- 2-(3-pyridinylmethyl)-, phenylmethyl ester

Base Information

Chemical Name:Hydrazinecarboxylic acid, 2-[[2-[(1,1-dimethylethoxy)carbonyl]-1-(2-methylpropyl)hydrazino]acetyl]- 2-(3-pyridinylmethyl)-, phenylmethyl ester
CAS No.:827337-67-7
Molecular Formula:C25H35N5O5
Molecular Weight:485.583
Hs Code.:

Hydrazinecarboxylic acid,
2-[[2-[(1,1-dimethylethoxy)carbonyl]-1-(2-methylpropyl)hydrazino]acetyl]-
2-(3-pyridinylmethyl)-, phenylmethyl ester

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Hydrazinecarboxylic acid, 2-[[2-[(1,1-dimethylethoxy)carbonyl]-1-(2-methylpropyl)hydrazino]acetyl]- 2-(3-pyridinylmethyl)-, phenylmethyl ester

Chemical Property:

Purity/Quality:

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Hazard Codes:

MSDS Files:: SDS file from LookChem

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Technology Process of Hydrazinecarboxylic acid, 2-[[2-[(1,1-dimethylethoxy)carbonyl]-1-(2-methylpropyl)hydrazino]acetyl]- 2-(3-pyridinylmethyl)-, phenylmethyl ester

There total 2 articles about Hydrazinecarboxylic acid, 2-[[2-[(1,1-dimethylethoxy)carbonyl]-1-(2-methylpropyl)hydrazino]acetyl]- 2-(3-pyridinylmethyl)-, phenylmethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 357953-50-5
(N'-tert-butoxycarbonyl-N-isobutyl-hydrazino)-acetic acid

: N^α-(pyridine-3-ylmethyl)-N^β-Z hydrazine

: 827337-67-7
N'-[2-(N'-benzyloxycarbonyl-N-pyridin-3-ylmethyl-hydrazino)-2-oxo-ethyl]-N'-isobutyl-hydrazinecarboxylic acid tert-butyl ester

Guidance literature:: With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; at 20 ℃; for 48h;
DOI:10.1021/jm049455f

Reference yield:

: 57699-53-3
N^α-isobutyl-N^β-Boc-hydrazine

: 827337-67-7
N'-[2-(N'-benzyloxycarbonyl-N-pyridin-3-ylmethyl-hydrazino)-2-oxo-ethyl]-N'-isobutyl-hydrazinecarboxylic acid tert-butyl ester

Guidance literature:: Multi-step reaction with 2 steps

1.1: methanol / 0.5 h / 20 °C

1.2: 90 percent / NaBH₃CN / methanol / 1 h

2.1: 70 percent / EDCI / CH₂Cl₂ / 48 h / 20 °C

With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In methanol; dichloromethane;
DOI:10.1021/jm049455f