1H-Pyrrole-2-carboxaldehyde, 5-(hydroxyphenylacetyl)-1-methyl-

Base Information

Chemical Name:1H-Pyrrole-2-carboxaldehyde, 5-(hydroxyphenylacetyl)-1-methyl-
CAS No.:828923-12-2
Molecular Formula:C14H13NO3
Molecular Weight:243.262
Hs Code.:
DSSTox Substance ID:DTXSID00465135

Synonyms:828923-12-2;1H-Pyrrole-2-carboxaldehyde, 5-(hydroxyphenylacetyl)-1-methyl-;DTXSID00465135;5-(2-hydroxy-2-phenylacetyl)-1-methyl-1h-pyrrole-2-carbaldehyde

Suppliers and Price of 1H-Pyrrole-2-carboxaldehyde, 5-(hydroxyphenylacetyl)-1-methyl-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 1 raw suppliers

Chemical Property of 1H-Pyrrole-2-carboxaldehyde, 5-(hydroxyphenylacetyl)-1-methyl-

Chemical Property:

XLogP3:1.5
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:4
Exact Mass:243.08954328
Heavy Atom Count:18
Complexity:312

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CN1C(=CC=C1C(=O)C(C2=CC=CC=C2)O)C=O

Technology Process of 1H-Pyrrole-2-carboxaldehyde, 5-(hydroxyphenylacetyl)-1-methyl-

There total 5 articles about 1H-Pyrrole-2-carboxaldehyde, 5-(hydroxyphenylacetyl)-1-methyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: N'-[5-(2-hydroxy-2-phenylacetyl)-1-methyl-1H-pyrrol-2-ylmethylene]-N,N,N-trimethylhydrazonium iodide

: 828923-12-2
5-(2-hydroxy-2-phenylacetyl)-1-methyl-1H-pyrrole-2-carbaldehyde

Guidance literature:: With hydrogenchloride; In water; at 50 ℃; for 1h;
DOI:10.1002/ejoc.200400293

Reference yield:

: 69819-66-5
N-methylpyrrole-2-carbaldehyde N,N-dimethylhydrazone

: 828923-12-2
5-(2-hydroxy-2-phenylacetyl)-1-methyl-1H-pyrrole-2-carbaldehyde

Guidance literature:: Multi-step reaction with 3 steps

1: 45 percent / O₂ / benzene / 1.5 h / 80 °C

2: 87 percent / acetonitrile / 24 h / 82 °C

3: 89 percent / aq. HCl / 1 h / Heating

With hydrogenchloride; oxygen; In acetonitrile; benzene;
DOI:10.1007/s10593-006-0025-2

Reference yield:

: 1075-06-5
2,2-dihydroxy-1-phenyl-ethanone

: 828923-12-2
5-(2-hydroxy-2-phenylacetyl)-1-methyl-1H-pyrrole-2-carbaldehyde

Guidance literature:: Multi-step reaction with 3 steps

1: 45 percent / O₂ / benzene / 1.5 h / 80 °C

2: 87 percent / acetonitrile / 24 h / 82 °C

3: 89 percent / aq. HCl / 1 h / Heating

With hydrogenchloride; oxygen; In acetonitrile; benzene;
DOI:10.1007/s10593-006-0025-2