5-[(But-3-en-2-yl)oxy]-1,3-dimethoxy-2-methylbenzene

Base Information

Chemical Name:5-[(But-3-en-2-yl)oxy]-1,3-dimethoxy-2-methylbenzene
CAS No.:831170-94-6
Molecular Formula:C13H18O3
Molecular Weight:222.284
Hs Code.:2909309090
DSSTox Substance ID:DTXSID80699653
Mol file:831170-94-6.mol

Synonyms:831170-94-6;5-[(But-3-en-2-yl)oxy]-1,3-dimethoxy-2-methylbenzene;DTXSID80699653

Suppliers and Price of 5-[(But-3-en-2-yl)oxy]-1,3-dimethoxy-2-methylbenzene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of 5-[(But-3-en-2-yl)oxy]-1,3-dimethoxy-2-methylbenzene

Chemical Property:

PSA：27.69000
LogP:2.96550
XLogP3:3.2
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:5
Exact Mass:222.125594432
Heavy Atom Count:16
Complexity:203

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC1=C(C=C(C=C1OC)OC(C)C=C)OC

Technology Process of 5-[(But-3-en-2-yl)oxy]-1,3-dimethoxy-2-methylbenzene

There total 2 articles about 5-[(But-3-en-2-yl)oxy]-1,3-dimethoxy-2-methylbenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 41.0%

: 598-32-3
2-hydroxy-3-butene

: 22080-97-3
3,5-dimethoxy-4-methylphenol

: 831170-94-6
1,3-dimethoxy-2-methyl-5-(1-methylallyloxy)benzene

Guidance literature:: With di-isopropyl azodicarboxylate; triphenylphosphine; In tetrahydrofuran; at 60 ℃;
DOI:10.1002/anie.200461294

Reference yield:

: 831171-37-0
(3,5-dimethoxy-4-methylphenoxy)triisopropylsilane

: 831170-94-6
1,3-dimethoxy-2-methyl-5-(1-methylallyloxy)benzene

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / HCl / ethanol; H₂O / 20 h / 23 °C

2: 41 percent / triphenylphosphine; diisopropyl azodicarboxylate / tetrahydrofuran / 60 °C

With hydrogenchloride; di-isopropyl azodicarboxylate; triphenylphosphine; In tetrahydrofuran; ethanol; water;
DOI:10.1002/anie.200461294