Benzenemethanamine, N-[2-phenyl-2-(phenylseleno)propylidene]-

Base Information

• Chemical Name: Benzenemethanamine, N-[2-phenyl-2-(phenylseleno)propylidene]-
• CAS No.: 831200-75-0
• Molecular Formula: C22H21NSe
• DSSTox Substance ID: DTXSID90479488

Synonyms:831200-75-0;Benzenemethanamine, N-[2-phenyl-2-(phenylseleno)propylidene]-;DTXSID90479488

Chemical Property of Benzenemethanamine, N-[2-phenyl-2-(phenylseleno)propylidene]-

Chemical Property:

• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 6
• Exact Mass: 379.08392
• Heavy Atom Count: 24
• Complexity: 375

Purity/Quality:

85.0-99.8% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Canonical SMILES: CC(C=NCC1=CC=CC=C1)(C2=CC=CC=C2)[Se]C3=CC=CC=C3

Technology Process of Benzenemethanamine, N-[2-phenyl-2-(phenylseleno)propylidene]-

There total 1 articles about Benzenemethanamine, N-[2-phenyl-2-(phenylseleno)propylidene]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-Phenyl-2-phenylselanyl-propionaldehyde (121034-40-0) + benzylamine (100-46-9) → phenyl-N-(2-phenyl-2-(phenylselanyl)propylidene)methanamine (831200-75-0)

Guidance literature:

In toluene; for 12h; Heating;

DOI:10.1016/j.tet.2004.10.065

Reference yield: 59.0%

phenyl-N-(2-phenyl-2-(phenylselanyl)propylidene)methanamine (831200-75-0) → N-benzyl-2-phenyl-2-(phenylselanyl)propan-1-amine (730907-47-8)

Guidance literature:

With sodium cyanoborohydride; acetic acid; In ethanol; at -78 ℃; for 1h;

DOI:10.1016/j.tet.2004.10.065

Reference yield: 47.0%

phenyl-N-(2-phenyl-2-(phenylselanyl)propylidene)methanamine (831200-75-0) + allylmagnesium bromide (2622-05-1) → 3-allyl-1-benzyl-2-methyl-2-phenylaziridine + N-benzyl-2-phenyl-2-(phenylselanyl)hex-5-en-3-amine

Guidance literature:

In tetrahydrofuran; at -40 - 0 ℃; for 2.5h;

DOI:10.1016/j.tet.2004.10.065

upstream raw materials:

2-Phenyl-2-phenylselanyl-propionaldehyde

benzylamine

Downstream raw materials:

N-benzyl-2-phenyl-2-(phenylselanyl)propan-1-amine

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