Benzenemethanamine, N-[1-phenyl-2-(phenylseleno)propylidene]-

Base Information

• Chemical Name: Benzenemethanamine, N-[1-phenyl-2-(phenylseleno)propylidene]-
• CAS No.: 831200-81-8
• Molecular Formula: C22H21NSe
• Molecular Weight: 378.375
• DSSTox Substance ID: DTXSID40473315

Synonyms:831200-81-8;Benzenemethanamine, N-[1-phenyl-2-(phenylseleno)propylidene]-;DTXSID40473315

Chemical Property of Benzenemethanamine, N-[1-phenyl-2-(phenylseleno)propylidene]-

Chemical Property:

• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 6
• Exact Mass: 379.08392
• Heavy Atom Count: 24
• Complexity: 373

Purity/Quality:

85.0-99.8% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC(C(=NCC1=CC=CC=C1)C2=CC=CC=C2)[Se]C3=CC=CC=C3

Technology Process of Benzenemethanamine, N-[1-phenyl-2-(phenylseleno)propylidene]-

There total 1 articles about Benzenemethanamine, N-[1-phenyl-2-(phenylseleno)propylidene]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-phenyl-2-(phenylselanyl)propanone (42858-33-3) + benzylamine (100-46-9) → phenyl-N-(1-phenyl-2-(phenylselanyl)propylidene)methanamine (831200-81-8)

Guidance literature:

With titanium tetrachloride; In diethyl ether; at 20 ℃; for 5h;

DOI:10.1016/S0040-4039(99)02159-0

Reference yield: 53.0%

phenyl-N-(1-phenyl-2-(phenylselanyl)propylidene)methanamine (831200-81-8) → N-benzyl-1-phenyl-2-(phenylselanyl)propan-1-amine

Guidance literature:

With sodium cyanoborohydride; acetic acid; In ethanol; at -78 ℃; for 1h;

DOI:10.1016/j.tet.2004.10.065

Reference yield: 41.0%

allylmagnesium bromide (2622-05-1) + phenyl-N-(1-phenyl-2-(phenylselanyl)propylidene)methanamine (831200-81-8) → 2-allyl-1-benzyl-3-methyl-2-phenylaziridine

Guidance literature:

In tetrahydrofuran; for 2h; Heating;

DOI:10.1016/j.tet.2004.10.065

upstream raw materials:

1-phenyl-2-(phenylselanyl)propanone

benzylamine

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