1,5(2H)-Pyrimidinedicarboxylic acid, 3,6-dihydro-4-methyl-6-(3-nitrophenyl)-2-oxo-, 5-(1-methylethyl) 1-[(1S)-1-methyl-2-[methyl(phenylmethyl)amino]ethyl] ester

Base Information

Chemical Name:1,5(2H)-Pyrimidinedicarboxylic acid, 3,6-dihydro-4-methyl-6-(3-nitrophenyl)-2-oxo-, 5-(1-methylethyl) 1-[(1S)-1-methyl-2-[methyl(phenylmethyl)amino]ethyl] ester
CAS No.:832075-56-6
Molecular Formula:C₂₇H₃₂N₄O₇
Molecular Weight:524.574
Hs Code.:

1,5(2H)-Pyrimidinedicarboxylic acid,
3,6-dihydro-4-methyl-6-(3-nitrophenyl)-2-oxo-, 5-(1-methylethyl)
1-[(1S)-1-methyl-2-[methyl(phenylmethyl)amino]ethyl] ester

Synonyms:

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Chemical Property of 1,5(2H)-Pyrimidinedicarboxylic acid, 3,6-dihydro-4-methyl-6-(3-nitrophenyl)-2-oxo-, 5-(1-methylethyl) 1-[(1S)-1-methyl-2-[methyl(phenylmethyl)amino]ethyl] ester

Chemical Property:

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Safty Information:

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MSDS Files:: SDS file from LookChem

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Technology Process of 1,5(2H)-Pyrimidinedicarboxylic acid, 3,6-dihydro-4-methyl-6-(3-nitrophenyl)-2-oxo-, 5-(1-methylethyl) 1-[(1S)-1-methyl-2-[methyl(phenylmethyl)amino]ethyl] ester

There total 7 articles about 1,5(2H)-Pyrimidinedicarboxylic acid, 3,6-dihydro-4-methyl-6-(3-nitrophenyl)-2-oxo-, 5-(1-methylethyl) 1-[(1S)-1-methyl-2-[methyl(phenylmethyl)amino]ethyl] ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2-Methoxy-4-methyl-6-(3-nitro-phenyl)-6H-pyrimidine-1,5-dicarboxylic acid 1-[(S)-2-(benzyl-methyl-amino)-1-methyl-ethyl] ester 5-isopropyl ester

: 832075-56-6
3,6-dihydro-4-methyl-6-(3-nitrophenyl)-2-oxo-1,5(2H)-pyrimidinedicarboxylic acid 5-(1-methylethyl) 1-<(S)-1-methyl-2-ethyl> diester

Guidance literature:: With hydrogenchloride; In tetrahydrofuran; for 2h;
DOI:10.1021/jm00095a023

Reference yield:

: 2-Methoxy-6-methyl-4-(3-nitro-phenyl)-1,4-dihydro-pyrimidine-5-carboxylic acid isobutyl ester

: 832075-56-6
3,6-dihydro-4-methyl-6-(3-nitrophenyl)-2-oxo-1,5(2H)-pyrimidinedicarboxylic acid 5-(1-methylethyl) 1-<(S)-1-methyl-2-ethyl> diester

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) pyridine / 1.) acetonitrile, toluene, RT, 1h, 2.) acetonitrile, toluene, RT, overnight

2: 2 N aq. HCl / tetrahydrofuran / 2 h

With pyridine; hydrogenchloride; In tetrahydrofuran;
DOI:10.1021/jm00095a023

Reference yield:

: (S)-1-(Benzyl-methyl-amino)-propan-2-ol; hydrochloride

: 832075-56-6
3,6-dihydro-4-methyl-6-(3-nitrophenyl)-2-oxo-1,5(2H)-pyrimidinedicarboxylic acid 5-(1-methylethyl) 1-<(S)-1-methyl-2-ethyl> diester

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) pyridine / 1.) acetonitrile, toluene, RT, 1h, 2.) acetonitrile, toluene, RT, overnight

2: 2 N aq. HCl / tetrahydrofuran / 2 h

With pyridine; hydrogenchloride; In tetrahydrofuran;
DOI:10.1021/jm00095a023