Benzo(b)thiophen-3-ol, 2-((4-fluorophenyl)azo)-4-methoxy-7-(10-methoxy-5-methyl-4,5,6,7-tetrahydro-3H-furo(4,3,2-fg)(3)benzazocin-6-yl)-, 1,1-dioxide

Base Information

• Chemical Name: Benzo(b)thiophen-3-ol, 2-((4-fluorophenyl)azo)-4-methoxy-7-(10-methoxy-5-methyl-4,5,6,7-tetrahydro-3H-furo(4,3,2-fg)(3)benzazocin-6-yl)-, 1,1-dioxide
• CAS No.: 155857-49-1
• Molecular Formula: C₂₉H₂₆FN₃O₆S
• Molecular Weight: 563.606
• Mol file: 155857-49-1.mol

Synonyms:155857-49-1;Benzo(b)thiophen-3-ol, 2-((4-fluorophenyl)azo)-4-methoxy-7-(10-methoxy-5-methyl-4,5,6,7-tetrahydro-3H-furo(4,3,2-fg)(3)benzazocin-6-yl)-, 1,1-dioxide;C29H26FN3O6S;C29-H26-F-N3-O6-S;LS-41277

Chemical Property of Benzo(b)thiophen-3-ol, 2-((4-fluorophenyl)azo)-4-methoxy-7-(10-methoxy-5-methyl-4,5,6,7-tetrahydro-3H-furo(4,3,2-fg)(3)benzazocin-6-yl)-, 1,1-dioxide

Chemical Property:

• Vapor Pressure: 0mmHg at 25°C
• Boiling Point: 780.3°Cat760mmHg
• Flash Point: 425.7°C
• Density: 1.48g/cm³
• XLogP3: 2.8
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 10
• Rotatable Bond Count: 5
• Exact Mass: 563.15263489
• Heavy Atom Count: 40
• Complexity: 1310

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC1CCC2C3=C1C(C=NC=C(C3=CO2)OC)C4=C5C(=C(C=C4)OC)C(=O)C(=NNC6=CC=C(C=C6)F)S5(=O)=O
• Isomeric SMILES: CC1CCC2C3=C1C(C=N/C=C(\C3=CO2)/OC)C4=C5C(=C(C=C4)OC)C(=O)/C(=N\NC6=CC=C(C=C6)F)/S5(=O)=O

Technology Process of Benzo(b)thiophen-3-ol, 2-((4-fluorophenyl)azo)-4-methoxy-7-(10-methoxy-5-methyl-4,5,6,7-tetrahydro-3H-furo(4,3,2-fg)(3)benzazocin-6-yl)-, 1,1-dioxide

There total 1 articles about Benzo(b)thiophen-3-ol, 2-((4-fluorophenyl)azo)-4-methoxy-7-(10-methoxy-5-methyl-4,5,6,7-tetrahydro-3H-furo(4,3,2-fg)(3)benzazocin-6-yl)-, 1,1-dioxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

4-fluorophenyldiazonium chloride (20893-71-4) + 10-methoxy-6(4'-methoxy-benzo-2'-hydrothiophen-3'-on-S,S-dioxido)-5-methyl-3,4,6,7-tetrahydro-5H-furo(4.3.2-fg)-(3)-benzazacine (107672-79-7,155857-35-5) → 2-(4-Fluoro-phenylazo)-4-methoxy-7-(3-methoxy-8-methyl-7,8,9,10-tetrahydro-6H-2-oxa-8-aza-cycloocta[cd]inden-7-yl)-1,1-dioxo-1H-1λ6-benzo[b]thiophen-3-ol (155857-49-1)

Guidance literature:

With pyridine; In water; at 0 - 20 ℃; for 0.5h;

DOI:10.1007/BF00780573

upstream raw materials:

4-fluorophenyldiazonium chloride

10-methoxy-6(4'-methoxy-benzo-2'-hydrothiophen-3'-on-S,S-dioxido)-5-methyl-3,4,6,7-tetrahydro-5H-furo(4.3.2-fg)-⁽³⁾-benzazacine