2-(Bromomethyl)-1-[(3-methoxyphenyl)methyl]aziridine

Base Information

Chemical Name:2-(Bromomethyl)-1-[(3-methoxyphenyl)methyl]aziridine
CAS No.:832724-75-1
Molecular Formula:C11H14BrNO
Molecular Weight:256.142
Hs Code.:
DSSTox Substance ID:DTXSID10465868

Synonyms:832724-75-1;2-(bromomethyl)-1-[(3-methoxyphenyl)methyl]aziridine;2-(bromomethyl)-1-(3-methoxybenzyl)aziridine;Aziridine, 2-(bromomethyl)-1-[(3-methoxyphenyl)methyl]-;DTXSID10465868;2-Bromomethyl-1-(3-methoxy-benzyl)-aziridine

Suppliers and Price of 2-(Bromomethyl)-1-[(3-methoxyphenyl)methyl]aziridine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of 2-(Bromomethyl)-1-[(3-methoxyphenyl)methyl]aziridine

Chemical Property:

XLogP3:2.3
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:4
Exact Mass:255.02588
Heavy Atom Count:14
Complexity:188

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC1=CC=CC(=C1)CN2CC2CBr

Technology Process of 2-(Bromomethyl)-1-[(3-methoxyphenyl)methyl]aziridine

There total 3 articles about 2-(Bromomethyl)-1-[(3-methoxyphenyl)methyl]aziridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: (2,3-Dibromo-propyl)-[1-(3-methoxy-phenyl)-meth-(E)-ylidene]-amine

: 832724-75-1
2-(bromomethyl)-1-[(3-methoxyphenyl)methyl]aziridine

Guidance literature:: With sodium tetrahydroborate; In methanol; for 2h; Heating;
DOI:10.1021/jo048486f

Reference yield:

: 591-31-1
3-methoxy-benzaldehyde

: 832724-75-1
2-(bromomethyl)-1-[(3-methoxyphenyl)methyl]aziridine

Guidance literature:: Multi-step reaction with 3 steps

1: 95 percent / magnesium sulfate / CH₂Cl₂ / 1 h / Heating

2: 100 percent / bromine / CH₂Cl₂ / 0.5 h / 20 °C

3: 81 percent / sodium borohydride / methanol / 2 h / Heating

With sodium tetrahydroborate; bromine; magnesium sulfate; In methanol; dichloromethane;
DOI:10.1021/jo048486f

Reference yield:

: 246509-60-4
N-[(3-methoxyphenyl)methylidene]-N-(2-propenyl)amine

: 832724-75-1
2-(bromomethyl)-1-[(3-methoxyphenyl)methyl]aziridine

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / bromine / CH₂Cl₂ / 0.5 h / 20 °C

2: 81 percent / sodium borohydride / methanol / 2 h / Heating

With sodium tetrahydroborate; bromine; In methanol; dichloromethane;
DOI:10.1021/jo048486f