3-Chloro-10,11-dihydro-5H-dibenzo(a,d)cycloheptene-5-carboxamide

Base Information

Chemical Name:3-Chloro-10,11-dihydro-5H-dibenzo(a,d)cycloheptene-5-carboxamide
CAS No.:67196-53-6
Molecular Formula:C16H14ClNO
Molecular Weight:271.7415
Hs Code.:
DSSTox Substance ID:DTXSID30986303
Nikkaji Number:J72.806C
Mol file:67196-53-6.mol

Synonyms:BRN 2589712;67196-53-6;3-Chloro-10,11-dihydro-5H-dibenzo(a,d)cycloheptene-5-carboxamide;5H-Dibenzo(a,d)cycloheptene-5-carboxamide, 10,11-dihydro-3-chloro-;DTXSID30986303;LS-60676;10,11-Dihydro-3-chloro-5H-dibenzo[a,d]cycloheptene-5-carboxamide;3-Chloro-10,11-dihydro-5H-dibenzo[a,d][7]annulene-5-carboximidic acid;5H-Dibenzo[a,d]cycloheptene-5-carboxamide, 3-chloro-10,11-dihydro-

Suppliers and Price of 3-Chloro-10,11-dihydro-5H-dibenzo(a,d)cycloheptene-5-carboxamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of 3-Chloro-10,11-dihydro-5H-dibenzo(a,d)cycloheptene-5-carboxamide

Chemical Property:

Vapor Pressure:1.79E-08mmHg at 25°C
Boiling Point:455.2°Cat760mmHg
Flash Point:229.1°C
PSA：44.08000
Density:1.268g/cm³
LogP:4.20550
XLogP3:3.4
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:1
Exact Mass:271.0763918
Heavy Atom Count:19
Complexity:346

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1CC2=CC=CC=C2C(C3=C1C=CC(=C3)Cl)C(=O)N

Technology Process of 3-Chloro-10,11-dihydro-5H-dibenzo(a,d)cycloheptene-5-carboxamide

There total 3 articles about 3-Chloro-10,11-dihydro-5H-dibenzo(a,d)cycloheptene-5-carboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 92435-50-2
3-chloro-10,11-dihydro-5H-dibenzo[a,d]cyclohepten-5-ol

: 67196-53-6
3-Chlor-dibenzocycloheptadien-5-carboxamid

Guidance literature:: Multi-step reaction with 3 steps

1: HCl / benzene

2: benzene

3: (i) BF₃, aq. AcOH, (ii) aq. NaOH

With hydrogenchloride; In benzene;
DOI:10.1021/jm00331a019

Reference yield:

: 54491-74-6
3,5-Dichlordibenzo1,4-cycloheptadien

: 67196-53-6
3-Chlor-dibenzocycloheptadien-5-carboxamid

Guidance literature:: Multi-step reaction with 2 steps

1: benzene

2: (i) BF₃, aq. AcOH, (ii) aq. NaOH

In benzene;
DOI:10.1021/jm00331a019