Technology Process of Benzene, [[[(2Z)-3-methyl-2-hexenyl]oxy]methyl]-
There total 4 articles about Benzene, [[[(2Z)-3-methyl-2-hexenyl]oxy]methyl]- which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
2(E)-(2-benzyloxyethylidene)pentan-1-ol;
With
sulfur trioxide pyridine complex;
In
tetrahydrofuran;
at 0 ℃;
for 3h;
With
lithium aluminium tetrahydride;
In
tetrahydrofuran;
for 25h;
DOI:10.1023/B:RUCB.0000035654.60768.fb
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: lithium diethylamide / tetrahydrofuran; hexane / -10 - 0 °C
1.2: tetrahydrofuran; hexane; hexamethylphosphoric acid triamide / -70 - 0 °C
1.3: 61 percent / hydrochloric acid / tetrahydrofuran; hexane; hexamethylphosphoric acid triamide / 3.5 h / 20 °C
2.1: 94 percent / sodium borohydride
3.1: pyridine-sulfur trioxide / tetrahydrofuran / 3 h / 0 °C
3.2: 67 percent / LiAlH4 / tetrahydrofuran / 25 h
With
sodium tetrahydroborate; lithium diethylamide; sulfur trioxide pyridine complex;
In
tetrahydrofuran; hexane;
DOI:10.1023/B:RUCB.0000035654.60768.fb
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: lithium diethylamide / tetrahydrofuran; hexane / -10 - 0 °C
1.2: tetrahydrofuran; hexane; hexamethylphosphoric acid triamide / -70 - 0 °C
1.3: 61 percent / hydrochloric acid / tetrahydrofuran; hexane; hexamethylphosphoric acid triamide / 3.5 h / 20 °C
2.1: 94 percent / sodium borohydride
3.1: pyridine-sulfur trioxide / tetrahydrofuran / 3 h / 0 °C
3.2: 67 percent / LiAlH4 / tetrahydrofuran / 25 h
With
sodium tetrahydroborate; lithium diethylamide; sulfur trioxide pyridine complex;
In
tetrahydrofuran; hexane;
DOI:10.1023/B:RUCB.0000035654.60768.fb
