2-Butyl-3-(4-hydroxybutyl)cyclohex-2-EN-1-one

Base Information

Chemical Name:2-Butyl-3-(4-hydroxybutyl)cyclohex-2-EN-1-one
CAS No.:83562-29-2
Molecular Formula:C14H24O2
Molecular Weight:224.33900
Hs Code.:
DSSTox Substance ID:DTXSID90556985
Wikidata:Q82438722

Synonyms:2-BUTYL-3-(4-HYDROXYBUTYL)CYCLOHEX-2-EN-1-ONE;83562-29-2;DTXSID90556985

Suppliers and Price of 2-Butyl-3-(4-hydroxybutyl)cyclohex-2-EN-1-one

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of 2-Butyl-3-(4-hydroxybutyl)cyclohex-2-EN-1-one

Chemical Property:

PSA：37.30000
LogP:3.38880
XLogP3:2.6
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:7
Exact Mass:224.177630004
Heavy Atom Count:16
Complexity:254

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCCCC1=C(CCCC1=O)CCCCO

Technology Process of 2-Butyl-3-(4-hydroxybutyl)cyclohex-2-EN-1-one

There total 5 articles about 2-Butyl-3-(4-hydroxybutyl)cyclohex-2-EN-1-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 88367-24-2
2-butyl-3-(4-tetrahydropyranyloxybutyl)cyclohex-2-enone

: 83562-29-2
2-Butyl-3-(4-hydroxybutyl)-2-cyclohexen-1-one

Guidance literature:: With pyridinium p-toluenesulfonate; In ethanol; at 60 ℃; for 5h;
DOI:10.1039/P19830002383

Reference yield:

: 928-51-8
4-Chloro-1-butanol

: 56459-18-8
2-butyl-3-ethoxy-2-cyclohexen-1-one

: 83562-29-2
2-Butyl-3-(4-hydroxybutyl)-2-cyclohexen-1-one

Guidance literature:: With magnesium; Yield given. Multistep reaction; 1.) THF, 2.) THF;
DOI:10.1021/jo00145a057

Reference yield:

: 6093-95-4
methyl 5-oxodecanoate

: 83562-29-2
2-Butyl-3-(4-hydroxybutyl)-2-cyclohexen-1-one

Guidance literature:: Multi-step reaction with 4 steps

1: 83 percent / t-BuOK / diethyl ether; 2-methyl-propan-2-ol / 5 h / Heating

2: 98 percent / toluene-p-sulphonic acid / benzene / 24 h / Heating

3: 1.) Mg, 1,2-dibromoethane / 1.) THF, -78 deg C, 30 min, 2.) room temperature, 15 h

4: 7.9 g / pyridinium toluene-p-sulphonate / ethanol / 5 h / 60 °C

With potassium tert-butylate; pyridinium p-toluenesulfonate; toluene-4-sulfonic acid; magnesium; ethylene dibromide; In diethyl ether; ethanol; tert-butyl alcohol; benzene;
DOI:10.1039/P19830002383