Methanone, (3-azido-4,6-dimethylthieno[2,3-b]pyridin-2-yl)phenyl-

Base Information

Chemical Name:Methanone, (3-azido-4,6-dimethylthieno[2,3-b]pyridin-2-yl)phenyl-
CAS No.:835626-21-6
Molecular Formula:C16H12N4OS
Molecular Weight:308.363
Hs Code.:
DSSTox Substance ID:DTXSID90477560
Wikidata:Q82310337

Synonyms:835626-21-6;Methanone, (3-azido-4,6-dimethylthieno[2,3-b]pyridin-2-yl)phenyl-;DTXSID90477560

Suppliers and Price of Methanone, (3-azido-4,6-dimethylthieno[2,3-b]pyridin-2-yl)phenyl-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 1 raw suppliers

Chemical Property of Methanone, (3-azido-4,6-dimethylthieno[2,3-b]pyridin-2-yl)phenyl-

Chemical Property:

XLogP3:5.6
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:3
Exact Mass:308.07318219
Heavy Atom Count:22
Complexity:473

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC(=NC2=C1C(=C(S2)C(=O)C3=CC=CC=C3)N=[N+]=[N-])C

Technology Process of Methanone, (3-azido-4,6-dimethylthieno[2,3-b]pyridin-2-yl)phenyl-

There total 2 articles about Methanone, (3-azido-4,6-dimethylthieno[2,3-b]pyridin-2-yl)phenyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 52505-58-5
3-amino-4,6-dimethyl-2-benzoylthieno<2,3-b>pyridine

: 835626-21-6
(3-azido-4,6-dimethyl-thieno[2,3-b]pyridin-2-yl)-phenyl-methanone

Guidance literature:: 3-amino-4,6-dimethyl-2-benzoylthieno<2,3-b>pyridine; With sulfuric acid; acetic acid; sodium nitrite; at 5 - 7 ℃;

With sodium azide;
DOI:10.1023/B:COHC.0000028636.31350.c0

Reference yield:

: 54585-47-6
4,6-Dimethyl-2-thioxo-1,2-dihydro-pyridine-3-carbonitrile

: 835626-21-6
(3-azido-4,6-dimethyl-thieno[2,3-b]pyridin-2-yl)-phenyl-methanone

Guidance literature:: Multi-step reaction with 2 steps

1.1: 89 percent / aq. KOH / dimethylformamide / 20 °C

2.1: H₂SO₄; aq. NaNO₂; glacial acetic acid / 5 - 7 °C

2.2: 78 percent / aq. NaN₃

With potassium hydroxide; sulfuric acid; acetic acid; sodium nitrite; In N,N-dimethyl-formamide;
DOI:10.1023/B:COHC.0000028636.31350.c0