Phosphoric acid, 2-[4-[4-[[[(1-acetyl-2,3-dihydro-5-methyl-7-nitro-1H-indol-4-yl)oxy]acetyl] amino]benzoyl]phenoxy]ethyl bis(1,1-dimethylethyl) ester

Base Information

Chemical Name:Phosphoric acid, 2-[4-[4-[[[(1-acetyl-2,3-dihydro-5-methyl-7-nitro-1H-indol-4-yl)oxy]acetyl] amino]benzoyl]phenoxy]ethyl bis(1,1-dimethylethyl) ester
CAS No.:835889-79-7
Molecular Formula:C36H44N3O11P
Molecular Weight:725.733
Hs Code.:

Phosphoric acid,
2-[4-[4-[[[(1-acetyl-2,3-dihydro-5-methyl-7-nitro-1H-indol-4-yl)oxy]acetyl]
amino]benzoyl]phenoxy]ethyl bis(1,1-dimethylethyl) ester

Synonyms:

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Chemical Property of Phosphoric acid, 2-[4-[4-[[[(1-acetyl-2,3-dihydro-5-methyl-7-nitro-1H-indol-4-yl)oxy]acetyl] amino]benzoyl]phenoxy]ethyl bis(1,1-dimethylethyl) ester

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Technology Process of Phosphoric acid, 2-[4-[4-[[[(1-acetyl-2,3-dihydro-5-methyl-7-nitro-1H-indol-4-yl)oxy]acetyl] amino]benzoyl]phenoxy]ethyl bis(1,1-dimethylethyl) ester

There total 14 articles about Phosphoric acid, 2-[4-[4-[[[(1-acetyl-2,3-dihydro-5-methyl-7-nitro-1H-indol-4-yl)oxy]acetyl] amino]benzoyl]phenoxy]ethyl bis(1,1-dimethylethyl) ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 770251-05-3
(1-acetyl-5-methyl-7-nitroindolin-4-yloxy)acetic acid

: 835889-69-5
phosphoric acid 2-[4-(4-amino-benzoyl)-phenoxy]-ethyl ester di-tert-butyl ester

: 835889-79-7
4-[(1-acetyl-5-methyl-7-nitroindolin-4-yloxy)acetamido]-4'-{2-[di(tert-butoxy)phosphoryloxy]ethoxy}benzophenone

Guidance literature:: With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In acetonitrile; at 20 ℃; for 18h;
DOI:10.1016/j.tet.2004.10.094

Reference yield:

: phosphorous acid di-tert-butyl ester 2-[4-(4-nitro-benzoyl)-phenoxy]-ethyl ester

: 835889-79-7
4-[(1-acetyl-5-methyl-7-nitroindolin-4-yloxy)acetamido]-4'-{2-[di(tert-butoxy)phosphoryloxy]ethoxy}benzophenone

Guidance literature:: Multi-step reaction with 3 steps

1: 0.77 g / m-chloroperbenzoic acid / CH₂Cl₂ / 1 h / 4 °C

2: H₂ / Pd/C / ethanol

3: 55 percent / 1-(3-dimethylaminopropyl)-3-ethylcarbodiimide hydrochloride / acetonitrile / 18 h / 20 °C

With hydrogen; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; 3-chloro-benzenecarboperoxoic acid; palladium on activated charcoal; In ethanol; dichloromethane; acetonitrile;
DOI:10.1016/j.tet.2004.10.094

Reference yield:

: 835889-68-4
4-{2-[di(tert-butoxy)phosphoryloxy]ethoxy}-4'-nitrobenzophenone

: 835889-79-7
4-[(1-acetyl-5-methyl-7-nitroindolin-4-yloxy)acetamido]-4'-{2-[di(tert-butoxy)phosphoryloxy]ethoxy}benzophenone

Guidance literature:: Multi-step reaction with 2 steps

1: H₂ / Pd/C / ethanol

2: 55 percent / 1-(3-dimethylaminopropyl)-3-ethylcarbodiimide hydrochloride / acetonitrile / 18 h / 20 °C

With hydrogen; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; palladium on activated charcoal; In ethanol; acetonitrile;
DOI:10.1016/j.tet.2004.10.094