4-Morpholineethanamine, N-(6-(3-chlorophenyl)-3-pyridazinyl)-, dihydrochloride

Base Information

• Chemical Name: 4-Morpholineethanamine, N-(6-(3-chlorophenyl)-3-pyridazinyl)-, dihydrochloride
• CAS No.: 118269-86-6
• Molecular Formula: C₁₇H₂₁ClN₄O*2ClH
• Molecular Weight: 405.755
• DSSTox Substance ID: DTXSID20152075

Synonyms:N-(6-(3-Chlorophenyl)-3-pyridazinyl)-4-morpholineethanamine dihydrochloride;4-Morpholineethanamine, N-(6-(3-chlorophenyl)-3-pyridazinyl)-, dihydrochloride;118269-86-6;DTXSID20152075;LS-92856

Chemical Property of 4-Morpholineethanamine, N-(6-(3-chlorophenyl)-3-pyridazinyl)-, dihydrochloride

Chemical Property:

• Vapor Pressure: 2.35E-12mmHg at 25°C
• Boiling Point: 554.9°Cat760mmHg
• Flash Point: 289.4°C
• Density: g/cm³
• Hydrogen Bond Donor Count: 3
• Hydrogen Bond Acceptor Count: 5
• Rotatable Bond Count: 5
• Exact Mass: 404.093744
• Heavy Atom Count: 25
• Complexity: 354

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC1=CC(=NN=C1NCCN2CCOCC2)C3=CC(=CC=C3)Cl.Cl.Cl

Technology Process of 4-Morpholineethanamine, N-(6-(3-chlorophenyl)-3-pyridazinyl)-, dihydrochloride

There total 2 articles about 4-Morpholineethanamine, N-(6-(3-chlorophenyl)-3-pyridazinyl)-, dihydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

6-(m-Chlorophenyl)-4-methyl-3(2H)-pyridazinone (28657-56-9) → [6-(3-Chloro-phenyl)-4-methyl-pyridazin-3-yl]-(2-morpholin-4-yl-ethyl)-amine; hydrochloride (118269-86-6)

Guidance literature:

Multi-step reaction with 2 steps

1: POCl₃ / 80 °C

With trichlorophosphate;

DOI:10.1021/jm00123a004

Reference yield:

4-(2-AMINOETHYL)MORPHOLINE (2038-03-1) + 3-chloro-6-(m-chlorophenyl)-4-methylpyridazine (28657-40-1) → [6-(3-Chloro-phenyl)-4-methyl-pyridazin-3-yl]-(2-morpholin-4-yl-ethyl)-amine; hydrochloride (118269-86-6)

Guidance literature:

DOI:10.1021/jm00123a004

upstream raw materials:

4-(2-AMINOETHYL)MORPHOLINE

3-chloro-6-(m-chlorophenyl)-4-methylpyridazine

6-(m-Chlorophenyl)-4-methyl-3(2H)-pyridazinone

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