O(4)-Butylthymidine

Base Information

• Chemical Name: O(4)-Butylthymidine
• CAS No.: 82543-41-7
• Molecular Formula: C14H22N2O5
• Molecular Weight: 0
• Mol file: 82543-41-7.mol

Synonyms:O4-butylthymidine;4-Butoxy-1-((2R,4S,5R)-4-hydroxy-5-hydroxymethyl-tetrahydro-furan-2-yl)-5-methyl-1H-pyrimidin-2-one;

Chemical Property of O(4)-Butylthymidine

Chemical Property:

• PSA: 93.81000
• LogP: 0.37130

Purity/Quality:

97% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of O(4)-Butylthymidine

There total 5 articles about O(4)-Butylthymidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

3',5'-di-O-acetyl-O4-(1H-triazol-1-yl)thymidine + butan-1-ol (71-36-3) → O4-butylthymidine (82543-41-7)

Guidance literature:

With sodium; at 20 ℃; for 1h;

DOI:10.1002/(SICI)1522-2675(19991215)82:12<2172::AID-HLCA2172>3.0.CO;2-R

Reference yield:

3',5'-di-O-acetyl-O4-butylthymidine → O4-butylthymidine (82543-41-7)

Guidance literature:

With ammonia; In methanol; at 20 ℃; for 15h;

DOI:10.1002/(SICI)1522-2675(19991215)82:12<2172::AID-HLCA2172>3.0.CO;2-R

Reference yield:

C26H50N2O5Si2 → O4-butylthymidine (82543-41-7)

Guidance literature:

With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 20 ℃;

DOI:10.1093/nar/gkv941

upstream raw materials:

butan-1-ol

1-((2R,4S,5R)-4-((tert-butyldimethylsilyl)oxy)-5-(((tertbutyldimethylsilyl)oxy)methyl)tetrahydrofuran-2-yl)-5-methyl-4-(1H-1,2,4-triazol-1-yl)pyrimidin-2(1H)-one

Downstream raw materials:

O⁴-butyl-5'-O-(4,4'-dimethoxytrityl)thymidine

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