2-Methyl-5-(phenoxymethyl)cyclohex-2-en-1-one

Base Information

Chemical Name:2-Methyl-5-(phenoxymethyl)cyclohex-2-en-1-one
CAS No.:84065-64-5
Molecular Formula:C14H16O2
Molecular Weight:216.28
Hs Code.:
DSSTox Substance ID:DTXSID20510873

Synonyms:2-Methyl-5-(phenoxymethyl)cyclohex-2-en-1-one;84065-64-5;DTXSID20510873

Suppliers and Price of 2-Methyl-5-(phenoxymethyl)cyclohex-2-en-1-one

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-Methyl-5-(phenoxymethyl)cyclohex-2-en-1-one

Chemical Property:

XLogP3:2.8
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:3
Exact Mass:216.115029749
Heavy Atom Count:16
Complexity:275

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CCC(CC1=O)COC2=CC=CC=C2

Technology Process of 2-Methyl-5-(phenoxymethyl)cyclohex-2-en-1-one

There total 3 articles about 2-Methyl-5-(phenoxymethyl)cyclohex-2-en-1-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 84065-62-3
5-(phenoxymethyl)-4-(phenylsulfonyl)-2-methylcyclohex-2-enone

: 84065-64-5
5-(phenoxymethyl)-2-methylcyclohex-2-en-1-one

Guidance literature:: With zinc; In acetic acid; for 20h; Ambient temperature;
DOI:10.1021/jo00173a040

Reference yield:

: 1746-13-0
allyl phenyl ether

: 84065-64-5
5-(phenoxymethyl)-2-methylcyclohex-2-en-1-one

Guidance literature:: Multi-step reaction with 3 steps

1: 2.) 15percent H₂O₂ / 1.) CCl₄, irradiation, 1.5 h, 2.) CH₂Cl₂, 30 min, 0 deg C then 30 min, RT

2: 2.) 1percent HCl / 1.) xylene, reflux, 20 h, 2.) THF, RT, 5 h

3: 63 percent / zinc dust / acetic acid / 20 h / Ambient temperature

With hydrogenchloride; dihydrogen peroxide; zinc; In acetic acid;
DOI:10.1021/jo00173a040

Reference yield:

: 77825-83-3
(E)-3-(Benzenesulfonyl)-2-propenyl phenyl ether

: 84065-64-5
5-(phenoxymethyl)-2-methylcyclohex-2-en-1-one

Guidance literature:: Multi-step reaction with 2 steps

1: 2.) 1percent HCl / 1.) xylene, reflux, 20 h, 2.) THF, RT, 5 h

2: 63 percent / zinc dust / acetic acid / 20 h / Ambient temperature

With hydrogenchloride; zinc; In acetic acid;
DOI:10.1021/jo00173a040