1H-Pyrrole-2-carboxylic acid, 3,4-bis[2-(acetyloxy)ethyl]-5-[(acetyloxy)methyl]-, phenylmethyl ester

Base Information

Chemical Name:1H-Pyrrole-2-carboxylic acid, 3,4-bis[2-(acetyloxy)ethyl]-5-[(acetyloxy)methyl]-, phenylmethyl ester
CAS No.:84089-83-8
Molecular Formula:C₂₃H₂₇NO₈
Molecular Weight:445.469
Hs Code.:

Synonyms:

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Chemical Property of 1H-Pyrrole-2-carboxylic acid, 3,4-bis[2-(acetyloxy)ethyl]-5-[(acetyloxy)methyl]-, phenylmethyl ester

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Technology Process of 1H-Pyrrole-2-carboxylic acid, 3,4-bis[2-(acetyloxy)ethyl]-5-[(acetyloxy)methyl]-, phenylmethyl ester

There total 10 articles about 1H-Pyrrole-2-carboxylic acid, 3,4-bis[2-(acetyloxy)ethyl]-5-[(acetyloxy)methyl]-, phenylmethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 50622-73-6
methyl 3-<(methoxycarbonyl)methyl>-5-methylpyrrole-2-carboxylate

: 84089-83-8
benzyl 3,4-di(2-acetoxyethyl)-5-acetoxymethylpyrrole-2-carboxylate

Guidance literature:: Multi-step reaction with 5 steps

1: 2.8 g / stannous chloride dihydrate / 1 h / Ambient temperature

2: 14.3 g / thallium(III) nitrate trihydrate, perchloric acid / methanol / 0.5 h / Ambient temperature

3: 13 g / sodium metal / 3 h / 100 - 110 °C / 30 Torr

4: 1.) diborane / 1.) THF, 60 deg C, 2.) pyridine, RT, overnight

5: 9.3 g / acetic acid / 2 h

With perchloric acid; thallium(III) nitrate trihydrate; sodium; tin(ll) chloride; diborane; In methanol; acetic acid;

Reference yield:

: 73869-95-1
methyl 4-acetyl-3-methoxycarbonylmethyl-5-methylpyrrole-2-carboxylate

: 84089-83-8
benzyl 3,4-di(2-acetoxyethyl)-5-acetoxymethylpyrrole-2-carboxylate

Guidance literature:: Multi-step reaction with 4 steps

1: 14.3 g / thallium(III) nitrate trihydrate, perchloric acid / methanol / 0.5 h / Ambient temperature

2: 13 g / sodium metal / 3 h / 100 - 110 °C / 30 Torr

3: 1.) diborane / 1.) THF, 60 deg C, 2.) pyridine, RT, overnight

4: 9.3 g / acetic acid / 2 h

With perchloric acid; thallium(III) nitrate trihydrate; sodium; diborane; In methanol; acetic acid;

Reference yield:

: 123-54-6,81235-32-7
acetylacetone

: 84089-83-8
benzyl 3,4-di(2-acetoxyethyl)-5-acetoxymethylpyrrole-2-carboxylate

Guidance literature:: Multi-step reaction with 5 steps

1: 1.) pentyl nitrite, HCl, 2.) acetic acid, ammonum acetate, zinc / 1.) from 40 deg C to RT, 2.) heating, 2 h

2: 14.3 g / thallium(III) nitrate trihydrate, perchloric acid / methanol / 0.5 h / Ambient temperature

3: 13 g / sodium metal / 3 h / 100 - 110 °C / 30 Torr

4: 1.) diborane / 1.) THF, 60 deg C, 2.) pyridine, RT, overnight

5: 9.3 g / acetic acid / 2 h

With hydrogenchloride; perchloric acid; thallium(III) nitrate trihydrate; n-Amyl nitrite; ammonium acetate; sodium; acetic acid; diborane; zinc; In methanol; acetic acid;