5-Amino-1-[5-carboxy-3,4-dihydro-2,4-dioxopyrimidin-1(2H)-yl]-1,5-dideoxy-β-D-allofuranuronic acid

Base Information

Chemical Name:5-Amino-1-[5-carboxy-3,4-dihydro-2,4-dioxopyrimidin-1(2H)-yl]-1,5-dideoxy-β-D-allofuranuronic acid
CAS No.:24695-46-3
Molecular Formula:C₁₁H₁₃N₃O₉
Molecular Weight:331.239
Hs Code.:
Mol file:24695-46-3.mol

Synonyms:5-Pyrimidinecarboxylicacid, 1-(5-amino-5-deoxy-b-D-allofuranuronosyl)-1,2,3,4-tetrahydro-2,4-dioxo- (8CI); Polyoxin C acid

Suppliers and Price of 5-Amino-1-[5-carboxy-3,4-dihydro-2,4-dioxopyrimidin-1(2H)-yl]-1,5-dideoxy-β-D-allofuranuronic acid

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of 5-Amino-1-[5-carboxy-3,4-dihydro-2,4-dioxopyrimidin-1(2H)-yl]-1,5-dideoxy-β-D-allofuranuronic acid

Chemical Property:

PSA：205.17000
LogP:-3.03380

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 5-Amino-1-[5-carboxy-3,4-dihydro-2,4-dioxopyrimidin-1(2H)-yl]-1,5-dideoxy-β-D-allofuranuronic acid

There total 7 articles about 5-Amino-1-[5-carboxy-3,4-dihydro-2,4-dioxopyrimidin-1(2H)-yl]-1,5-dideoxy-β-D-allofuranuronic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1-[(2R,3R,4S,5R)-5-((S)-Benzyloxycarbonylamino-carboxy-methyl)-3,4-dihydroxy-tetrahydro-furan-2-yl]-2,4-dioxo-1,2,3,4-tetrahydro-pyrimidine-5-carboxylic acid

: 24695-46-3
5-carboxy-1-(5'-amino-5'-deoxy-β-D-allofuranosyluronic acid)uracil

Guidance literature:: With hydrogen; palladium on activated charcoal; In methanol; at 20 ℃;

Reference yield:

: 155154-68-0
methyl (5-azido-5-deoxy-1,2,3-tri-O-acetyl-D-allofuranosid)uronate

: 24695-46-3
5-carboxy-1-(5'-amino-5'-deoxy-β-D-allofuranosyluronic acid)uracil

Guidance literature:: Multi-step reaction with 5 steps

1: trimethylsilyl trifluoromethanesulfonate / acetonitrile / 1 h / Heating

2: H₂ / Pd-C / ethyl acetate / 20 °C

3: NaHCO₃ / toluene; dioxane / 0.5 h / 20 °C

4: LiOH*H₂O / tetrahydrofuran; H₂O / 10 h / 0 °C

5: H₂ / Pd-C / methanol / 20 °C

With lithium hydroxide; trimethylsilyl trifluoromethanesulfonate; hydrogen; sodium hydrogencarbonate; palladium on activated charcoal; In tetrahydrofuran; 1,4-dioxane; methanol; water; ethyl acetate; toluene; acetonitrile;

Reference yield:

: 111052-06-3
ethyl 2,4-bis(trimethylsiloxy)pyrimidine-5-carboxylate

: 24695-46-3
5-carboxy-1-(5'-amino-5'-deoxy-β-D-allofuranosyluronic acid)uracil

Guidance literature:: Multi-step reaction with 5 steps

1: trimethylsilyl trifluoromethanesulfonate / acetonitrile / 1 h / Heating

2: H₂ / Pd-C / ethyl acetate / 20 °C

3: NaHCO₃ / toluene; dioxane / 0.5 h / 20 °C

4: LiOH*H₂O / tetrahydrofuran; H₂O / 10 h / 0 °C

5: H₂ / Pd-C / methanol / 20 °C

With lithium hydroxide; trimethylsilyl trifluoromethanesulfonate; hydrogen; sodium hydrogencarbonate; palladium on activated charcoal; In tetrahydrofuran; 1,4-dioxane; methanol; water; ethyl acetate; toluene; acetonitrile;