1,1,3,3-Tetrachloro-2,2,4,4-tetramethylcyclobutane

Base Information

• Chemical Name: 1,1,3,3-Tetrachloro-2,2,4,4-tetramethylcyclobutane
• CAS No.: 7374-59-6
• Molecular Formula: C8H12Cl4
• Molecular Weight: 249.9929
• NSC Number: 135921
• DSSTox Substance ID: DTXSID00300315
• Wikidata: Q82043275

Synonyms:1,1,3,3-tetrachloro-2,2,4,4-tetramethylcyclobutane;7374-59-6;NSC 135921;NSC135921;DTXSID00300315;NSC-135921

Chemical Property of 1,1,3,3-Tetrachloro-2,2,4,4-tetramethylcyclobutane

Chemical Property:

• Vapor Pressure: 0.0255mmHg at 25°C
• Boiling Point: 255.9°Cat760mmHg
• Flash Point: 101.7°C
• Density: 1.31g/cm³
• XLogP3: 4.7
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 0
• Rotatable Bond Count: 0
• Exact Mass: 249.966361
• Heavy Atom Count: 12
• Complexity: 171

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC1(C(C(C1(Cl)Cl)(C)C)(Cl)Cl)C

Technology Process of 1,1,3,3-Tetrachloro-2,2,4,4-tetramethylcyclobutane

There total 3 articles about 1,1,3,3-Tetrachloro-2,2,4,4-tetramethylcyclobutane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

2,2,4,4-tetramethyl-1,3-cyclobutanedione (933-52-8) → 1,1,3,3-tetrachloro-2,2,4,4-tetramethylcyclobutane (7374-59-6)

Guidance literature:

With phosphorus pentachloride; In tetrachloromethane; for 4h; Heating;

Reference yield: 59.0%

2,2,4,4-tetramethyl-1,3-cyclobutanedione (933-52-8) → 1,1,3,3-tetrachloro-2,2,4,4-tetramethylcyclobutane (7374-59-6) + 3,3-dichloro-2,2,4,4-tetramethylcyclobutan-1-one (633303-45-4)

Guidance literature:

With phosphorus pentachloride; In tetrachloromethane; for 1.5h; Heating;

DOI:10.1002/hlca.200590203

Reference yield:

→ 1,1,3,3-tetrachloro-2,2,4,4-tetramethylcyclobutane (7374-59-6)

Guidance literature:

Tetramethylcyclobutandion, PCl5;

DOI:10.1021/jo01023a550

upstream raw materials:

2,2,4,4-tetramethyl-1,3-cyclobutanedione

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