Technology Process of 2-(2,6-Diethyl-4-azidophenylimino)imidazolidine
There total 5 articles about 2-(2,6-Diethyl-4-azidophenylimino)imidazolidine which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 69.9 percent / POCl3 / 3 h / Heating
2: 91.1 percent / H2O / 3 h / Heating
3: 1.) NaNO2, AcOH, 2.) 35percent HNO3 / 1.) H2O, 5 deg C, 1.5 h, 2.) a) 5 deg C, 0.5 h, b) reflux, 1 h
4: Fe, HCl / ethanol; H2O / 0.5 h / Heating
5: 1.) NaNO2, AcOH, 2.) NaN3 / 1.) H2O, 4 deg C, 3 min, 2.) H2O, 2-4 deg C, 10 min
With
hydrogenchloride; sodium azide; water; nitric acid; iron; acetic acid; sodium nitrite; trichlorophosphate;
In
ethanol; water;
DOI:10.1021/jm00128a022
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 91.1 percent / H2O / 3 h / Heating
2: 1.) NaNO2, AcOH, 2.) 35percent HNO3 / 1.) H2O, 5 deg C, 1.5 h, 2.) a) 5 deg C, 0.5 h, b) reflux, 1 h
3: Fe, HCl / ethanol; H2O / 0.5 h / Heating
4: 1.) NaNO2, AcOH, 2.) NaN3 / 1.) H2O, 4 deg C, 3 min, 2.) H2O, 2-4 deg C, 10 min
With
hydrogenchloride; sodium azide; water; nitric acid; iron; acetic acid; sodium nitrite;
In
ethanol; water;
DOI:10.1021/jm00128a022
- Guidance literature:
-
Multi-step reaction with 2 steps
1: Fe, HCl / ethanol; H2O / 0.5 h / Heating
2: 1.) NaNO2, AcOH, 2.) NaN3 / 1.) H2O, 4 deg C, 3 min, 2.) H2O, 2-4 deg C, 10 min
With
hydrogenchloride; sodium azide; iron; acetic acid; sodium nitrite;
In
ethanol; water;
DOI:10.1021/jm00128a022