2-(2,6-Diethyl-4-azidophenylimino)imidazolidine

Base Information

Chemical Name:2-(2,6-Diethyl-4-azidophenylimino)imidazolidine
CAS No.:121158-53-0
Molecular Formula:C₁₃H₁₈N₆
Molecular Weight:258.326
Hs Code.:
DSSTox Substance ID:DTXSID50153171
Nikkaji Number:J613.301K
Wikidata:Q83020025
ChEMBL ID:CHEMBL300893
Mol file:121158-53-0.mol

Synonyms:2-((4-azido-2,6-diethylphenyl)imino)imidazolidine;2-(2,6-diethyl-4-azidophenylimino)imidazolidine;NC 5Z;NC-5Z

Suppliers and Price of 2-(2,6-Diethyl-4-azidophenylimino)imidazolidine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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Total 0 raw suppliers

Chemical Property of 2-(2,6-Diethyl-4-azidophenylimino)imidazolidine

Chemical Property:

Boiling Point:°Cat760mmHg
Flash Point:°C
PSA：86.17000
Density:g/cm³
LogP:2.41446
XLogP3:3.1
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:5
Exact Mass:258.15929460
Heavy Atom Count:19
Complexity:359

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCC1=CC(=CC(=C1NC2=NCCN2)CC)N=[N+]=[N-]

Technology Process of 2-(2,6-Diethyl-4-azidophenylimino)imidazolidine

There total 5 articles about 2-(2,6-Diethyl-4-azidophenylimino)imidazolidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 579-66-8
2,6-diethylaniline

: 121158-53-0
N-(4-azido-2,6-diethylphenyl)-4,5-dihydro-1H-imidazol-2(3H)-imine

Guidance literature:: Multi-step reaction with 5 steps

1: 69.9 percent / POCl₃ / 3 h / Heating

2: 91.1 percent / H₂O / 3 h / Heating

3: 1.) NaNO₂, AcOH, 2.) 35percent HNO₃ / 1.) H₂O, 5 deg C, 1.5 h, 2.) a) 5 deg C, 0.5 h, b) reflux, 1 h

4: Fe, HCl / ethanol; H₂O / 0.5 h / Heating

5: 1.) NaNO₂, AcOH, 2.) NaN₃ / 1.) H₂O, 4 deg C, 3 min, 2.) H₂O, 2-4 deg C, 10 min

With hydrogenchloride; sodium azide; water; nitric acid; iron; acetic acid; sodium nitrite; trichlorophosphate; In ethanol; water;
DOI:10.1021/jm00128a022

Reference yield:

: 86861-31-6
1-acetyl-N-(2,6-diethylphenyl)-4,5-dihydro-1H-imidazol-2(3H)-imine

: 121158-53-0
N-(4-azido-2,6-diethylphenyl)-4,5-dihydro-1H-imidazol-2(3H)-imine

Guidance literature:: Multi-step reaction with 4 steps

1: 91.1 percent / H₂O / 3 h / Heating

2: 1.) NaNO₂, AcOH, 2.) 35percent HNO₃ / 1.) H₂O, 5 deg C, 1.5 h, 2.) a) 5 deg C, 0.5 h, b) reflux, 1 h

3: Fe, HCl / ethanol; H₂O / 0.5 h / Heating

4: 1.) NaNO₂, AcOH, 2.) NaN₃ / 1.) H₂O, 4 deg C, 3 min, 2.) H₂O, 2-4 deg C, 10 min

With hydrogenchloride; sodium azide; water; nitric acid; iron; acetic acid; sodium nitrite; In ethanol; water;
DOI:10.1021/jm00128a022

Reference yield:

: 86861-32-7
N-(2,6-diethyl-4-nitrophenyl)-4,5-dihydro-1H-imidazol-2(3H)-imine

: 121158-53-0
N-(4-azido-2,6-diethylphenyl)-4,5-dihydro-1H-imidazol-2(3H)-imine

Guidance literature:: Multi-step reaction with 2 steps

1: Fe, HCl / ethanol; H₂O / 0.5 h / Heating

2: 1.) NaNO₂, AcOH, 2.) NaN₃ / 1.) H₂O, 4 deg C, 3 min, 2.) H₂O, 2-4 deg C, 10 min

With hydrogenchloride; sodium azide; iron; acetic acid; sodium nitrite; In ethanol; water;
DOI:10.1021/jm00128a022