7H-Pyrrolo[2,3-d]pyrimidin-2-amine, 4-chloro-5-[2-[[(1,1-dimethylethyl)diphenylsilyl]oxy]ethyl]-7-[(4-methoxy-3 ,5-dimethyl-2-pyridinyl)methyl]-

Base Information

• Chemical Name: 7H-Pyrrolo[2,3-d]pyrimidin-2-amine, 4-chloro-5-[2-[[(1,1-dimethylethyl)diphenylsilyl]oxy]ethyl]-7-[(4-methoxy-3 ,5-dimethyl-2-pyridinyl)methyl]-
• CAS No.: 848694-72-4
• Molecular Formula: C33H38ClN5O2Si
• Molecular Weight: 600.236

Synonyms:

Chemical Property of 7H-Pyrrolo[2,3-d]pyrimidin-2-amine, 4-chloro-5-[2-[[(1,1-dimethylethyl)diphenylsilyl]oxy]ethyl]-7-[(4-methoxy-3 ,5-dimethyl-2-pyridinyl)methyl]-

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Technology Process of 7H-Pyrrolo[2,3-d]pyrimidin-2-amine, 4-chloro-5-[2-[[(1,1-dimethylethyl)diphenylsilyl]oxy]ethyl]-7-[(4-methoxy-3 ,5-dimethyl-2-pyridinyl)methyl]-

There total 1 articles about 7H-Pyrrolo[2,3-d]pyrimidin-2-amine, 4-chloro-5-[2-[[(1,1-dimethylethyl)diphenylsilyl]oxy]ethyl]-7-[(4-methoxy-3 ,5-dimethyl-2-pyridinyl)methyl]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N-[5-[2-(tert-butyl-diphenyl-silanyloxy)-ethyl]-4-chloro-7-(4-methoxy-3,5-dimethyl-pyridin-2-ylmethyl)-7H-pyrrolo[2,3-d]pyrimidin-2-yl]-acetamide (848694-71-3) → 5-[2-(tert-butyl-diphenyl-silanyloxy)-ethyl]-4-chloro-7-(4-methoxy-3,5-dimethyl-pyridin-2-ylmethyl)-7H-pyrrolo[2,3-d]pyrimidin-2-ylamine (848694-72-4)

Guidance literature:

With methanol; sodium hydroxide; water; In tetrahydrofuran; at 45 ℃; for 1.5h;

Reference yield: 74.0%

5-[2-(tert-butyl-diphenyl-silanyloxy)-ethyl]-4-chloro-7-(4-methoxy-3,5-dimethyl-pyridin-2-ylmethyl)-7H-pyrrolo[2,3-d]pyrimidin-2-ylamine (848694-72-4) → 2-[2-amino-4-chloro-7-(4-methoxy-3,5-dimethyl-pyridin-2-ylmethyl)-7H-pyrrolo[2,3-d]pyrimidin-5-yl]-ethanol (848694-73-5)

Guidance literature:

With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 20 ℃; for 1h;

upstream raw materials:

N-[5-[2-(tert-butyl-diphenyl-silanyloxy)-ethyl]-4-chloro-7-(4-methoxy-3,5-dimethyl-pyridin-2-ylmethyl)-7H-pyrrolo[2,3-d]pyrimidin-2-yl]-acetamide

Downstream raw materials:

2-[2-amino-4-chloro-7-(4-methoxy-3,5-dimethyl-pyridin-2-ylmethyl)-7H-pyrrolo[2,3-d]pyrimidin-5-yl]-ethanol

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