(NZ)-N-(3-ethoxycyclohex-2-en-1-ylidene)hydroxylamine

Base Information

Chemical Name:(NZ)-N-(3-ethoxycyclohex-2-en-1-ylidene)hydroxylamine
CAS No.:7467-13-2
Molecular Formula:C8H13NO2
Molecular Weight:155.197
Hs Code.:
NSC Number:400649
DSSTox Substance ID:DTXSID60420982

Synonyms:NSC400649;7467-13-2;SCHEMBL16888162;DTXSID60420982;NSC-400649

Suppliers and Price of (NZ)-N-(3-ethoxycyclohex-2-en-1-ylidene)hydroxylamine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 7 raw suppliers

Chemical Property of (NZ)-N-(3-ethoxycyclohex-2-en-1-ylidene)hydroxylamine

Chemical Property:

Vapor Pressure:0.000125mmHg at 25°C
Boiling Point:298.7°Cat760mmHg
Flash Point:134.5°C
Density:1.1g/cm³
XLogP3:1.2
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:2
Exact Mass:155.094628657
Heavy Atom Count:11
Complexity:185

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCOC1=CC(=NO)CCC1
Isomeric SMILES:CCOC1=C/C(=N\O)/CCC1

Technology Process of (NZ)-N-(3-ethoxycyclohex-2-en-1-ylidene)hydroxylamine

There total 1 articles about (NZ)-N-(3-ethoxycyclohex-2-en-1-ylidene)hydroxylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

: 5323-87-5
3-Ethoxycyclohex-2-en-1-one

: 7467-13-2
3-ethoxy-2-cyclohexen-1-one oxime

Guidance literature:: With hydroxylamine hydrochloride; In ethanol; at 100 ℃; for 2h;

Reference yield: 87.0%

: 7467-13-2
3-ethoxy-2-cyclohexen-1-one oxime

: 165257-04-5
4-ethoxy-6,7-dihydro-1H-azepin-2(5H)-one

Guidance literature:: With methanesulfonyl chloride; triethylamine; In dichloromethane; at 0 ℃;
DOI:10.1021/ol900709n

Reference yield:

: 7467-13-2
3-ethoxy-2-cyclohexen-1-one oxime

: 1-(3-chlorophenyl)-4-ethoxy-6,7-dihydro-1H-azepin-2(5H)-one

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine; p-toluenesulfonyl chloride / tetrahydrofuran / 1 h / 0 - 5 °C

2: potassium carbonate; copper(l) iodide; N,N`-dimethylethylenediamine / 1,4-dioxane / 12 h / 140 °C / Inert atmosphere

With copper(l) iodide; potassium carbonate; triethylamine; p-toluenesulfonyl chloride; N,N`-dimethylethylenediamine; In tetrahydrofuran; 1,4-dioxane;