Carbamic acid, [2-[[(1,1-dimethylethoxy)carbonyl]methylamino]ethyl]methyl-, 2,4,6-tris[[[(1,1-dimethylethyl)dimethylsilyl]oxy]methyl]phenyl ester

Base Information

Chemical Name:Carbamic acid, [2-[[(1,1-dimethylethoxy)carbonyl]methylamino]ethyl]methyl-, 2,4,6-tris[[[(1,1-dimethylethyl)dimethylsilyl]oxy]methyl]phenyl ester
CAS No.:848826-52-8
Molecular Formula:C37H72N2O7Si3
Molecular Weight:741.244
Hs Code.:

Carbamic acid,
[2-[[(1,1-dimethylethoxy)carbonyl]methylamino]ethyl]methyl-,
2,4,6-tris[[[(1,1-dimethylethyl)dimethylsilyl]oxy]methyl]phenyl ester

Synonyms:

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Chemical Property of Carbamic acid, [2-[[(1,1-dimethylethoxy)carbonyl]methylamino]ethyl]methyl-, 2,4,6-tris[[[(1,1-dimethylethyl)dimethylsilyl]oxy]methyl]phenyl ester

Chemical Property:

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Technology Process of Carbamic acid, [2-[[(1,1-dimethylethoxy)carbonyl]methylamino]ethyl]methyl-, 2,4,6-tris[[[(1,1-dimethylethyl)dimethylsilyl]oxy]methyl]phenyl ester

There total 7 articles about Carbamic acid, [2-[[(1,1-dimethylethoxy)carbonyl]methylamino]ethyl]methyl-, 2,4,6-tris[[[(1,1-dimethylethyl)dimethylsilyl]oxy]methyl]phenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 848826-50-6
carbonic acid 4-nitro-phenyl ester 2,4,6-tris-(tert-butyl-dimethyl-silanyloxymethyl)-phenyl ester

: 112257-19-9
tert-butyl N-methyl-N-<2-(methylamino)ethyl>carbamate

: 848826-52-8
methyl-(2-{methyl-[2,4,6-tris-(tert-butyl-dimethyl-silanyloxymethyl)-phenoxycarbonyl]-amino}-ethyl)-carbamic acid tert-butyl ester

Guidance literature:: In N,N-dimethyl-formamide; at 20 ℃; for 0.666667h;

Reference yield:

: 848826-46-0
2,6-bis-(tert-butyl-dimethyl-silanyloxymethyl)-4-hydroxymethyl-phenol

: 848826-52-8
methyl-(2-{methyl-[2,4,6-tris-(tert-butyl-dimethyl-silanyloxymethyl)-phenoxycarbonyl]-amino}-ethyl)-carbamic acid tert-butyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 79 percent / dimethylformamide / 0.5 h / 20 °C

2: 94 percent / 4-(dimethylamino)pyridine; triethylamine / ethyl acetate / 1 h / 20 °C

3: 88 percent / dimethylformamide / 0.67 h / 20 °C

With dmap; triethylamine; In ethyl acetate; N,N-dimethyl-formamide;

Reference yield:

: 848826-44-8
3,5-bis-(tert-butyl-dimethyl-silanyloxymethyl)-4-hydroxy-benzoic acid ethyl ester

: 848826-52-8
methyl-(2-{methyl-[2,4,6-tris-(tert-butyl-dimethyl-silanyloxymethyl)-phenoxycarbonyl]-amino}-ethyl)-carbamic acid tert-butyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 75 percent / diisobutylaluminium hydride / dimethylformamide / 2 h / -78 °C

2: 79 percent / dimethylformamide / 0.5 h / 20 °C

3: 94 percent / 4-(dimethylamino)pyridine; triethylamine / ethyl acetate / 1 h / 20 °C

4: 88 percent / dimethylformamide / 0.67 h / 20 °C

With dmap; diisobutylaluminium hydride; triethylamine; In ethyl acetate; N,N-dimethyl-formamide;