(3-nitrophenyl)(4-nitrophenyl)arsinic acid

Base Information

• Chemical Name: (3-nitrophenyl)(4-nitrophenyl)arsinic acid
• CAS No.: 6339-86-2
• Molecular Formula: C₁₂H₉AsN₂O₆
• Molecular Weight: 352.135
• Mol file: 6339-86-2.mol

Synonyms:NSC 42501

Chemical Property of (3-nitrophenyl)(4-nitrophenyl)arsinic acid

Chemical Property:

• Vapor Pressure: 8.55E-15mmHg at 25°C
• Boiling Point: 590.6°Cat760mmHg
• Flash Point: 248°C
• Density: g/cm³

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of (3-nitrophenyl)(4-nitrophenyl)arsinic acid

There total 1 articles about (3-nitrophenyl)(4-nitrophenyl)arsinic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(4-nitro-phenyl)-phenyl-arsinic acid (18789-52-1) → (3-nitro-phenyl)-(4-nitro-phenyl)-arsinic acid (6339-86-2)

Guidance literature:

With sulfuric acid; nitric acid;

DOI:10.1021/ja01282a030

Reference yield:

(3-nitro-phenyl)-(4-nitro-phenyl)-arsinic acid (6339-86-2) → (3-amino-phenyl)-(4-amino-phenyl)-arsinic acid (6973-89-3)

Guidance literature:

With sodium hydroxide; iron(II) sulfate;

DOI:10.1021/ja01282a030

Reference yield:

(3-nitro-phenyl)-(4-nitro-phenyl)-arsinic acid (6339-86-2) → (3-hydroxy-phenyl)-(4-hydroxy-phenyl)-arsinic acid

Guidance literature:

Multi-step reaction with 2 steps

1: iron (II)-sulfate; aq. NaOH solution

2: aqueous sulfuric acid; sodium nitrite / anschliessend Erwaermen

With sodium hydroxide; sulfuric acid; iron(II) sulfate; sodium nitrite;

DOI:10.1021/ja01282a030

upstream raw materials:

(4-nitro-phenyl)-phenyl-arsinic acid

Downstream raw materials:

(3-amino-phenyl)-(4-amino-phenyl)-arsinic acid