Ethanone, 1-[4-[[1-[(acetyloxy)methyl]-1-methyl-2-propenyl]oxy]phenyl]-

Base Information

Chemical Name:Ethanone, 1-[4-[[1-[(acetyloxy)methyl]-1-methyl-2-propenyl]oxy]phenyl]-
CAS No.:850312-54-8
Molecular Formula:C15H18O4
Molecular Weight:262.306
Hs Code.:
DSSTox Substance ID:DTXSID20466604

Synonyms:850312-54-8;Ethanone, 1-[4-[[1-[(acetyloxy)methyl]-1-methyl-2-propenyl]oxy]phenyl]-;DTXSID20466604

Suppliers and Price of Ethanone, 1-[4-[[1-[(acetyloxy)methyl]-1-methyl-2-propenyl]oxy]phenyl]-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Total 1 raw suppliers

Chemical Property of Ethanone, 1-[4-[[1-[(acetyloxy)methyl]-1-methyl-2-propenyl]oxy]phenyl]-

Chemical Property:

XLogP3:2.3
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:7
Exact Mass:262.12050905
Heavy Atom Count:19
Complexity:342

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(=O)C1=CC=C(C=C1)OC(C)(COC(=O)C)C=C

Technology Process of Ethanone, 1-[4-[[1-[(acetyloxy)methyl]-1-methyl-2-propenyl]oxy]phenyl]-

There total 3 articles about Ethanone, 1-[4-[[1-[(acetyloxy)methyl]-1-methyl-2-propenyl]oxy]phenyl]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 108-24-7
acetic anhydride

: 850312-50-4
1-[4-(1-hydroxymethyl-1-methyl-allyloxy)-phenyl]-ethanone

: 850312-54-8
acetic acid 2-(4-acetyl-phenoxy)-2-methyl-but-3-enyl ester

Guidance literature:: With dmap; triethylamine; In ethyl acetate; at 20 ℃; for 4h;
DOI:10.1016/j.tetasy.2005.01.011

Reference yield:

: 1838-94-4
isoprene epoxide

: 850312-54-8
acetic acid 2-(4-acetyl-phenoxy)-2-methyl-but-3-enyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 95 percent / Pd(PPh₃) / CH₂Cl₂ / 4 h / 20 °C

2: 98 percent / Et₃N; DMAP / ethyl acetate / 4 h / 20 °C

With dmap; triethylamine; Pd(PPh₃); In dichloromethane; ethyl acetate;
DOI:10.1016/j.tetasy.2005.01.011

Reference yield:

: 99-93-4
4-Hydroxyacetophenone

: 850312-54-8
acetic acid 2-(4-acetyl-phenoxy)-2-methyl-but-3-enyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 95 percent / Pd(PPh₃) / CH₂Cl₂ / 4 h / 20 °C

2: 98 percent / Et₃N; DMAP / ethyl acetate / 4 h / 20 °C

With dmap; triethylamine; Pd(PPh₃); In dichloromethane; ethyl acetate;
DOI:10.1016/j.tetasy.2005.01.011