Cyclohexanecarbonitrile, 4-amino-1-(3-methoxyphenyl)-, cis-

Base Information

Chemical Name:Cyclohexanecarbonitrile, 4-amino-1-(3-methoxyphenyl)-, cis-
CAS No.:850885-66-4
Molecular Formula:C14H18N2O
Molecular Weight:230.31
Hs Code.:

Synonyms:

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Chemical Property of Cyclohexanecarbonitrile, 4-amino-1-(3-methoxyphenyl)-, cis-

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Technology Process of Cyclohexanecarbonitrile, 4-amino-1-(3-methoxyphenyl)-, cis-

There total 4 articles about Cyclohexanecarbonitrile, 4-amino-1-(3-methoxyphenyl)-, cis- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 850885-64-2
cis-4-[(diphenylmethyl)amino]-1-(3-methoxyphenyl)-cyclohexanecarbonitrile

: 850885-66-4
cis-4-amino-1-(3-methoxyphenyl)-cyclohexanecarbonitrile

Guidance literature:: With ammonium formate; palladium 10% on activated carbon; In ethanol; at 20 ℃; Heating / reflux;

Reference yield:

: methyl 5-cyano-2-hydroxy-5-(3-methoxyphenyl)cyclohexa-1-en-1-carboxylate

: 850885-66-4
cis-4-amino-1-(3-methoxyphenyl)-cyclohexanecarbonitrile

Guidance literature:: Multi-step reaction with 3 steps

1: water / dimethylsulfoxide-d6 / 9 h / 20 - 127 °C

2: sodium tris(acetoxy)borohydride / 1,2-dichloro-ethane / 0 - 20 °C

3: ammonium formate / palladium 10% on activated carbon / ethanol / 20 °C / Heating / reflux

With water; ammonium formate; sodium tris(acetoxy)borohydride; palladium 10% on activated carbon; In dimethylsulfoxide-d6; ethanol; 1,2-dichloro-ethane;

Reference yield:

: 19924-43-7
3-methoxyphenylacetonitrile

: 850885-66-4
cis-4-amino-1-(3-methoxyphenyl)-cyclohexanecarbonitrile

Guidance literature:: Multi-step reaction with 4 steps

1: sodium hydride / N,N-dimethyl-formamide / 2 h / 0 - 20 °C

2: water / dimethylsulfoxide-d6 / 9 h / 20 - 127 °C

3: sodium tris(acetoxy)borohydride / 1,2-dichloro-ethane / 0 - 20 °C

4: ammonium formate / palladium 10% on activated carbon / ethanol / 20 °C / Heating / reflux

With water; ammonium formate; sodium tris(acetoxy)borohydride; sodium hydride; palladium 10% on activated carbon; In dimethylsulfoxide-d6; ethanol; 1,2-dichloro-ethane; N,N-dimethyl-formamide;