1H-Imidazol-1-yloxy, 4-(dimethylamino)-2-ethyl-2,5-dihydro-5,5-dimethyl-2-[4-(phenylmethoxy )phenyl]-

Base Information

Chemical Name:1H-Imidazol-1-yloxy, 4-(dimethylamino)-2-ethyl-2,5-dihydro-5,5-dimethyl-2-[4-(phenylmethoxy )phenyl]-
CAS No.:851705-88-9
Molecular Formula:C22H28N3O2
Molecular Weight:366.483
Hs Code.:

Synonyms:

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Chemical Property of 1H-Imidazol-1-yloxy, 4-(dimethylamino)-2-ethyl-2,5-dihydro-5,5-dimethyl-2-[4-(phenylmethoxy )phenyl]-

Chemical Property:

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Technology Process of 1H-Imidazol-1-yloxy, 4-(dimethylamino)-2-ethyl-2,5-dihydro-5,5-dimethyl-2-[4-(phenylmethoxy )phenyl]-

There total 7 articles about 1H-Imidazol-1-yloxy, 4-(dimethylamino)-2-ethyl-2,5-dihydro-5,5-dimethyl-2-[4-(phenylmethoxy )phenyl]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2-(4-benzyloxy-phenyl)-4-dimethylamino-2-ethyl-5,5-dimethyl-2,5-dihydro-imidazol-1-ol

: 851705-88-9
C₂₂H₂₈N₃O₂

Guidance literature:: With manganese(IV) oxide; In tetrahydrofuran; for 2h;
DOI:10.1039/b418707e

Reference yield:

: 851705-73-2
2-(4-benzyloxy-phenyl)-4,5,5-trimethyl-2,5-dihydro-imidazol-1-ol

: 851705-88-9
C₂₂H₂₈N₃O₂

Guidance literature:: Multi-step reaction with 6 steps

1: 90 percent / PbO₂ / CH₂Cl₂

2: 80 percent / i-Pr-ONa; isopropyl nitrite / propan-2-ol / 20 °C

3: 90 percent / TsCl; Et₃N / CHCl₃ / 1 h

4: 90 percent / CH₂Cl₂ / 20 °C

5: tetrahydrofuran / 0.5 h

6: MnO₂ / tetrahydrofuran; various solvent(s) / 2 h

With manganese(IV) oxide; i-propyl nitrite; sodium isopropylate; lead dioxide; triethylamine; p-toluenesulfonyl chloride; In tetrahydrofuran; dichloromethane; chloroform; isopropyl alcohol;
DOI:10.1039/b418707e

Reference yield:

: 1026926-68-0
2-(4-benzyloxy-phenyl)-4,4,5-trimethyl-4H-imidazole 3-oxide

: 851705-88-9
C₂₂H₂₈N₃O₂

Guidance literature:: Multi-step reaction with 5 steps

1: 80 percent / i-Pr-ONa; isopropyl nitrite / propan-2-ol / 20 °C

2: 90 percent / TsCl; Et₃N / CHCl₃ / 1 h

3: 90 percent / CH₂Cl₂ / 20 °C

4: tetrahydrofuran / 0.5 h

5: MnO₂ / tetrahydrofuran; various solvent(s) / 2 h

With manganese(IV) oxide; i-propyl nitrite; sodium isopropylate; triethylamine; p-toluenesulfonyl chloride; In tetrahydrofuran; dichloromethane; chloroform; isopropyl alcohol;
DOI:10.1039/b418707e