Carbamic acid, propyl[[4-(3,3,4,4,5,5,6,6,7,7,8,8,8-tridecafluorooctyl)phenyl]methyl]-, 1,1-dimethylethyl ester

Base Information

Chemical Name:Carbamic acid, propyl[[4-(3,3,4,4,5,5,6,6,7,7,8,8,8-tridecafluorooctyl)phenyl]methyl]-, 1,1-dimethylethyl ester
CAS No.:852054-11-6
Molecular Formula:C23H26F13NO2
Molecular Weight:595.444
Hs Code.:

Synonyms:

Suppliers and Price of Carbamic acid, propyl[[4-(3,3,4,4,5,5,6,6,7,7,8,8,8-tridecafluorooctyl)phenyl]methyl]-, 1,1-dimethylethyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of Carbamic acid, propyl[[4-(3,3,4,4,5,5,6,6,7,7,8,8,8-tridecafluorooctyl)phenyl]methyl]-, 1,1-dimethylethyl ester

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of Carbamic acid, propyl[[4-(3,3,4,4,5,5,6,6,7,7,8,8,8-tridecafluorooctyl)phenyl]methyl]-, 1,1-dimethylethyl ester

There total 5 articles about Carbamic acid, propyl[[4-(3,3,4,4,5,5,6,6,7,7,8,8,8-tridecafluorooctyl)phenyl]methyl]-, 1,1-dimethylethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: propyl-[4-(3,3,4,4,5,5,6,6,7,7,8,8,8-tridecafluoro-oct-1-enyl)-benzyl]-carbamic acid tert-butyl ester

: 852054-11-6
propyl-[4-(3,3,4,4,5,5,6,6,7,7,8,8,8-tridecafluoro-octyl)-benzyl]-carbamic acid tert-butyl ester

Guidance literature:: With hydrogen; palladium on activated charcoal; In ethyl acetate; at 20 ℃; for 24h; under 2327.17 - 2585.74 Torr;
DOI:10.1021/jo048051s

Reference yield:

: 152300-61-3
tert-butyl (4-bromobenzyl)propylcarbamate

: 852054-11-6
propyl-[4-(3,3,4,4,5,5,6,6,7,7,8,8,8-tridecafluoro-octyl)-benzyl]-carbamic acid tert-butyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 66 percent / Bu₃N; n-Bu₄NHSO₄; NaOAc / Pd(OAc)2 / dimethylformamide / 40 h / Heating

2: 93 percent / H₂ / Pd/C / ethyl acetate / 24 h / 20 °C / 2327.17 - 2585.74 Torr

With tributyl-amine; hydrogen; sodium acetate; tetra(n-butyl)ammonium hydrogensulfate; palladium diacetate; palladium on activated charcoal; In ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1021/jo048051s

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 852054-11-6
propyl-[4-(3,3,4,4,5,5,6,6,7,7,8,8,8-tridecafluoro-octyl)-benzyl]-carbamic acid tert-butyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 100 percent / triethylamine / CH₂Cl₂ / 4.5 h / 20 °C

2: 66 percent / Bu₃N; n-Bu₄NHSO₄; NaOAc / Pd(OAc)2 / dimethylformamide / 40 h / Heating

3: 93 percent / H₂ / Pd/C / ethyl acetate / 24 h / 20 °C / 2327.17 - 2585.74 Torr

With tributyl-amine; hydrogen; sodium acetate; tetra(n-butyl)ammonium hydrogensulfate; triethylamine; palladium diacetate; palladium on activated charcoal; In dichloromethane; ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1021/jo048051s