1,3,2-Diazaphosphetidin-4-one, 2,2,2-trichloro-2,2-dihydro-1,3-dimethyl-

Base Information

• Chemical Name: 1,3,2-Diazaphosphetidin-4-one, 2,2,2-trichloro-2,2-dihydro-1,3-dimethyl-
• CAS No.: 3576-20-3
• Molecular Formula: C3H6Cl3N2OP
• Molecular Weight: 223.4253
• NSC Number: 203250
• DSSTox Substance ID: DTXSID90189292
• Wikidata: Q83061327

Synonyms:3576-20-3;1,3,2-Diazaphosphetidin-4-one, 2,2,2-trichloro-2,2-dihydro-1,3-dimethyl-;NSC203250;DTXSID90189292;NSC 203250;NSC-203250;1,3,2-Diazaphosphetidin-4-one,2,2,2-trichloro-2,2-dihydro-1,3-dimethyl-

Chemical Property of 1,3,2-Diazaphosphetidin-4-one, 2,2,2-trichloro-2,2-dihydro-1,3-dimethyl-

Chemical Property:

• Boiling Point: °Cat760mmHg
• Flash Point: °C
• Density: g/cm³
• XLogP3: 2
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 0
• Exact Mass: 221.928333
• Heavy Atom Count: 10
• Complexity: 184

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CN1C(=O)N(P1(Cl)(Cl)Cl)C

Technology Process of 1,3,2-Diazaphosphetidin-4-one, 2,2,2-trichloro-2,2-dihydro-1,3-dimethyl-

There total 2 articles about 1,3,2-Diazaphosphetidin-4-one, 2,2,2-trichloro-2,2-dihydro-1,3-dimethyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

N,N'-Dimethylurea (96-31-1) → 2,2,2-trichloro-1,3-dimethyl-1,3,2-diazaphosphetidin-4-one (3576-20-3)

Guidance literature:

With phosphorus pentachloride; In tetrachloromethane; Heating;

DOI:10.1007/BF00959653

Reference yield:

→ 2,2,2-trichloro-1,3-dimethyl-1,3,2-diazaphosphetidin-4-one (3576-20-3)

Guidance literature:

1,3-Dimethyl-harnstoff, Phosphor(V)-chlorid, CCl4, Δ; Nebenprodukt: Chlorameisensaeure--chlorid;

Reference yield: 20.0%

2,2,2-trichloro-1,3-dimethyl-1,3,2-diazaphosphetidin-4-one (3576-20-3) + bis(diphenyl)urea (102-07-8) → 4-Chlor-1,3-dimethyl-5,7-diphenyl-1,3,5,7-tetraaza-4λ5-phosphaspiro<3.3>heptan-2,6-dion (80049-55-4)

Guidance literature:

In dichloromethane; for 48h;

upstream raw materials:

N,N'-Dimethylurea

Downstream raw materials:

4-Chlor-1,3-dimethyl-5,7-diphenyl-1,3,5,7-tetraaza-4λ⁵-phosphaspiro<3.3>heptan-2,6-dion

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