2-Propenamide, N-[(4-hydroxy-3-methoxyphenyl)methyl]-

Base Information

Chemical Name:2-Propenamide, N-[(4-hydroxy-3-methoxyphenyl)methyl]-
CAS No.:852923-26-3
Molecular Formula:C11H13NO3
Molecular Weight:207.22600
Hs Code.:

Synonyms:2-Propenamide,N-[(4-hydroxy-3-methoxyphenyl)methyl];N-(4-hydroxy-3-methoxybenzyl)acrylamide;

Suppliers and Price of 2-Propenamide, N-[(4-hydroxy-3-methoxyphenyl)methyl]-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-Propenamide, N-[(4-hydroxy-3-methoxyphenyl)methyl]-

Chemical Property:

PSA：62.05000
LogP:2.04330

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 2-Propenamide, N-[(4-hydroxy-3-methoxyphenyl)methyl]-

There total 5 articles about 2-Propenamide, N-[(4-hydroxy-3-methoxyphenyl)methyl]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 41.0%

: 1196-92-5
Vanillylamin

: 814-68-6,25189-84-8
acryloyl chloride

: 852923-26-3
N-(4-hydroxy-3-methoxybenzyl)acrylamide

Guidance literature:: With triethylamine; In tetrahydrofuran; at 20 ℃; Inert atmosphere; Cooling with ice;
DOI:10.1016/j.polymer.2011.02.046

Reference yield: 31.0%

: 924-42-5,26374-25-4
N-Methylolacrylamid

: 90-05-1
2-methoxy-phenol

: 852923-26-3
N-(4-hydroxy-3-methoxybenzyl)acrylamide

Guidance literature:: With sulfuric acid; In ethanol; at 35 ℃; Cooling with ice;
DOI:10.1016/j.polymer.2011.02.046

Reference yield:

: 2874-33-1
vanillin oxime

: 852923-26-3
N-(4-hydroxy-3-methoxybenzyl)acrylamide

Guidance literature:: Multi-step reaction with 3 steps

1: hydrogenchloride; palladium 10% on activated carbon; hydrogen / ethanol / 3 h / 20 °C

2: sodium hydroxide / water

3: triethylamine / tetrahydrofuran / 20 °C / Inert atmosphere; Cooling with ice

With hydrogenchloride; palladium 10% on activated carbon; hydrogen; triethylamine; sodium hydroxide; In tetrahydrofuran; ethanol; water;
DOI:10.1016/j.polymer.2011.02.046