N-(3'-Morpholinopropyl)-2-norbornene-5,6-dicarboximide

Base Information

• Chemical Name: N-(3'-Morpholinopropyl)-2-norbornene-5,6-dicarboximide
• CAS No.: 74039-16-0
• Molecular Formula: C₁₆H₂₂N₂O₃
• Molecular Weight: 290.362
• NSC Number: 221684
• DSSTox Substance ID: DTXSID80995420
• Nikkaji Number: J83.688E
• Mol file: 74039-16-0.mol

Synonyms:74039-16-0;N-(3'-Morpholinopropyl)-2-norbornene-5,6-dicarboximide;NSC 221684;BRN 0037155;NSC221684;2-Norbornene-5,6-dicarboximide, N-(3-morpholinopropyl)-;2-[3-(morpholin-4-yl)propyl]-3a,4,7,7a-tetrahydro-1h-4,7-methanoisoindole-1,3(2h)-dione;DTXSID80995420;NSC-221684;4,7-Methano-1H-isoindole-1,3(2H)-dione, 3a,4,7,7a-tetrahydro-2-(3-(4-morpholinyl)propyl)-;2-Norbornene-5, N-(3-morpholinopropyl)-;WLN: T C555 A DVNV IUTJ E3- BT6N DOTJ;4,3(2H)-dione, 3a,4,7,7a-tetrahydro-2-[3-(4-morpholinyl)propyl]-

Chemical Property of N-(3'-Morpholinopropyl)-2-norbornene-5,6-dicarboximide

Chemical Property:

• Vapor Pressure: 2.31E-09mmHg at 25°C
• Boiling Point: 479.7°Cat760mmHg
• Flash Point: 243.9°C
• PSA: 49.85000
• Density: 1.233g/cm³
• LogP: 0.39160
• XLogP3: 0.3
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 4
• Rotatable Bond Count: 4
• Exact Mass: 290.16304257
• Heavy Atom Count: 21
• Complexity: 454

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1COCCN1CCCN2C(=O)C3C4CC(C3C2=O)C=C4

Technology Process of N-(3'-Morpholinopropyl)-2-norbornene-5,6-dicarboximide

There total 2 articles about N-(3'-Morpholinopropyl)-2-norbornene-5,6-dicarboximide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-(3-Aminopropyl)morpholine (123-00-2) + 3,6-endomethylene-1,2,3,6-tetrahydrophthalic anhydride (129-64-6) → 2-(3-morpholino-propyl)-(3ac,7ac)-3a,4,7,7a-tetrahydro-4r,7c-methano-isoindole-1,3-dione (74039-16-0)

Guidance literature:

Erhitzen des Reaktionsprodukts auf 170grad;

DOI:10.1021/ja01116a010

Reference yield:

→ 2-(3-morpholin-4-yl-propyl)-3a,4,7,7a-tetrahydro-4,7-methano-isoindole-1,3-dione (74039-16-0)

Guidance literature:

Anhydrid, Amin;

Reference yield:

2-(3-morpholino-propyl)-(3ac,7ac)-3a,4,7,7a-tetrahydro-4r,7c-methano-isoindole-1,3-dione (74039-16-0) → 2-(3-morpholino-propyl)-(3ar,7ac)-2,3,3a,4,7,7a-hexahydro-1H-4r,7c-methano-isoindole (73855-76-2)

Guidance literature:

With lithium aluminium tetrahydride; diethyl ether;

DOI:10.1021/ja01116a010

upstream raw materials:

4-(3-Aminopropyl)morpholine

3,6-endomethylene-1,2,3,6-tetrahydrophthalic anhydride

Downstream raw materials:

2-(3-morpholino-propyl)-(3ar,7ac)-2,3,3a,4,7,7a-hexahydro-1H-4r,7c-methano-isoindole

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