3-Oxa-5,9,11-triazatridecan-13-oic acid, 7-hydroxy-2,2-dimethyl-9-(1-methylethyl)-12-(2-methylpropyl)-4,10-dioxo -6-(phenylmethyl)-, methyl ester, (6R,7R,12R)-

Base Information

Chemical Name:3-Oxa-5,9,11-triazatridecan-13-oic acid, 7-hydroxy-2,2-dimethyl-9-(1-methylethyl)-12-(2-methylpropyl)-4,10-dioxo -6-(phenylmethyl)-, methyl ester, (6R,7R,12R)-
CAS No.:853905-00-7
Molecular Formula:C₂₆H₄₃N₃O₆
Molecular Weight:493.644
Hs Code.:

3-Oxa-5,9,11-triazatridecan-13-oic acid,
7-hydroxy-2,2-dimethyl-9-(1-methylethyl)-12-(2-methylpropyl)-4,10-dioxo
-6-(phenylmethyl)-, methyl ester, (6R,7R,12R)-

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-Oxa-5,9,11-triazatridecan-13-oic acid, 7-hydroxy-2,2-dimethyl-9-(1-methylethyl)-12-(2-methylpropyl)-4,10-dioxo -6-(phenylmethyl)-, methyl ester, (6R,7R,12R)-

Chemical Property:

Purity/Quality:

Safty Information:

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Hazard Codes:

MSDS Files:: SDS file from LookChem

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Technology Process of 3-Oxa-5,9,11-triazatridecan-13-oic acid, 7-hydroxy-2,2-dimethyl-9-(1-methylethyl)-12-(2-methylpropyl)-4,10-dioxo -6-(phenylmethyl)-, methyl ester, (6R,7R,12R)-

There total 4 articles about 3-Oxa-5,9,11-triazatridecan-13-oic acid, 7-hydroxy-2,2-dimethyl-9-(1-methylethyl)-12-(2-methylpropyl)-4,10-dioxo -6-(phenylmethyl)-, methyl ester, (6R,7R,12R)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 5845-53-4,6322-53-8,7517-19-3
(R)-leucine methyl ester hydrochloride

: 853905-00-7
(R)-2-[3-((2R,3R)-3-tert-Butoxycarbonylamino-2-hydroxy-4-phenyl-butyl)-3-isopropyl-ureido]-4-methyl-pentanoic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: NaHCO₃ / CH₂Cl₂; toluene / 0.5 h

2: CH₂Cl₂ / 6 h

With sodium hydrogencarbonate; In dichloromethane; toluene;
DOI:10.1021/jm049566e

Reference yield:

: 244092-76-0
(R)-N-(tert-butoxycarbonyl)-3-amino-4-phenyl-1-butene

: 853905-00-7
(R)-2-[3-((2R,3R)-3-tert-Butoxycarbonylamino-2-hydroxy-4-phenyl-butyl)-3-isopropyl-ureido]-4-methyl-pentanoic acid methyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: m-chloroperbenzoic acid / CH₂Cl₂

2: propan-2-ol / 12 h / Heating

3: CH₂Cl₂ / 6 h

With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; isopropyl alcohol;
DOI:10.1021/jm049566e

Reference yield:

: 156474-22-5
tert-butyl [(2R,3S)]-(-)-(1-oxiranyl-2-phenylethyl)carbamate

: 853905-00-7
(R)-2-[3-((2R,3R)-3-tert-Butoxycarbonylamino-2-hydroxy-4-phenyl-butyl)-3-isopropyl-ureido]-4-methyl-pentanoic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: propan-2-ol / 12 h / Heating

2: CH₂Cl₂ / 6 h

In dichloromethane; isopropyl alcohol;
DOI:10.1021/jm049566e