Ethyl 2-methyl-5-nitrofuran-3-carboxylate

Base Information

Chemical Name:Ethyl 2-methyl-5-nitrofuran-3-carboxylate
CAS No.:68967-34-0
Molecular Formula:C8H9NO5
Molecular Weight:199.1608
Hs Code.:
NSC Number:170611
DSSTox Substance ID:DTXSID80305383
Wikidata:Q82052010

Synonyms:ethyl 2-methyl-5-nitrofuran-3-carboxylate;68967-34-0;NSC170611;DTXSID80305383;NSC-170611

Suppliers and Price of Ethyl 2-methyl-5-nitrofuran-3-carboxylate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of Ethyl 2-methyl-5-nitrofuran-3-carboxylate

Chemical Property:

Vapor Pressure:0.00243mmHg at 25°C
Boiling Point:287.8°C at 760 mmHg
Flash Point:127.8°C
Density:1.287g/cm³
XLogP3:1.8
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:3
Exact Mass:199.04807239
Heavy Atom Count:14
Complexity:236

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCOC(=O)C1=C(OC(=C1)[N+](=O)[O-])C

Technology Process of Ethyl 2-methyl-5-nitrofuran-3-carboxylate

There total 3 articles about Ethyl 2-methyl-5-nitrofuran-3-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

: 141-97-9
ethyl acetoacetate

: 147591-81-9
5-methoxy[1,2,5]oxadiazolo[3,4-d]pyrimidine 1-oxide

: 68967-34-0
2-methyl-5-nitro-furan-3-carboxylic acid ethyl ester

Guidance literature:: With triethylamine; In dichloromethane; for 20h;
DOI:10.1007/BF02253048

Reference yield:

: 28921-35-9
2-methyl-3-ethoxycarbonyl-furan

: 68967-34-0
2-methyl-5-nitro-furan-3-carboxylic acid ethyl ester

Guidance literature:: With nitric acid; acetic anhydride; at -25 ℃;

Reference yield:

: 141-97-9
ethyl acetoacetate

: 68967-34-0
2-methyl-5-nitro-furan-3-carboxylic acid ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: aq. NaOH solution

2: nitric acid; acetic acid anhydride / -25 °C

With sodium hydroxide; nitric acid; acetic anhydride;